Citation: ZHAO Bo-Sheng, SHI Hui-Hu, MA Liang, DU Hong, ZHANG Jian-Bin. Preparation and CO₂ Adsorption Property of Flake-like Nano-Structure CeO₂ Crystals[J]. Chinese Journal of Inorganic Chemistry, ;2019, 35(1): 116-124. doi: 10.11862/CJIC.2019.019 shu

Preparation and CO₂ Adsorption Property of Flake-like Nano-Structure CeO₂ Crystals

ZHAO Bo-Sheng ^1,2 ,
SHI Hui-Hu ^1,2 ,
MA Liang ^1,2 ,
DU Hong ^1,2 ,
ZHANG Jian-Bin ^1,2,,

1.
College of Chemical Engineering, Inner Mongolia University of Technology, Hohhot 010051, China
2.
Inner Mongolia Engineering Research Center for CO₂ Capture and Utilization, Hohhot 010051, China

Corresponding author: ZHANG Jian-Bin, tadzhang@pku.edu.cn
Received Date: 30 August 2018
Revised Date: 26 November 2018

Figures(13)

Nano-structure flake-like CeO₂ crystals with an average size of 4.94 μm×0.92 μm (length and width) and the thickness of 0.04~0.08 μm were prepared by simply calcining cerium carbonate precursors (CCPs) at 500℃ for 4 h, in which the flake-like CCPs were firstly prepared by stirring CeCl₃ aqueous solution with CO₂-storage material (CO₂SM) for 0.5 h at room temperature. Interesting, the CO₂SM could provide CO₃^2- and act as dispersant and structure-directing agent for the preparation of flake-like CCPs. In the process, the effect of three factors, including CO₂SM dosage, Ce³⁺ concentration and stirring time, on the morphology and size of CCPs were systemically studied, and the optimum preparation conditions of flake-like CCPs were confirmed at 0.1 g CO₂SM with 50 mL 0.03 mol·L^-1 Ce³⁺ aqueous solution at 1 000 r·min^-1 for 0.5 h at room temperature. After calcining CCPs, the as-prepared flake-like CeO₂ crystals presented the CO₂ adsorption amount of 0.554 mmol·g^-1 at room temperature.
- CeO₂ crystals,
- cerium carbonate precursors,
- CO₂-storage material,
- CO₂ adsorption
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沈阳化工大学材料科学与工程学院沈阳 110142

Preparation and CO2 Adsorption Property of Flake-like Nano-Structure CeO2 Crystals

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通讯作者: 陈斌, bchen63@163.com

Preparation and CO₂ Adsorption Property of Flake-like Nano-Structure CeO₂ Crystals