Citation: ZHAO Meng-Jie, ZOU Xiang-Yu, XIA Yu-Hang, JIA Wen-Tao, ZHANG Hong-Bo, SHAO Jing, SU Chun-Hui. Preparation and Luminescence Properties of Ho³⁺-Yb³⁺ Co-doped Phosphate Glass-Ceramics[J]. Chinese Journal of Inorganic Chemistry, ;2019, 35(1): 95-100. doi: 10.11862/CJIC.2019.007 shu

Preparation and Luminescence Properties of Ho³⁺-Yb³⁺ Co-doped Phosphate Glass-Ceramics

1.
School of Material Science and Engineering, Changchun University of Science and Technology, Changchun 130022, China
2.
Changchun Normal University, Changchun 130032, China

Corresponding author: ZHANG Hong-Bo, zhb5388460@126.com
Received Date: 22 September 2018
Revised Date: 15 October 2018

Figures(9)

The Na₂O-Y₂O₃-P₂O₅-SiO₂ precursor glass was prepared by traditional melting method. The transparent phosphate glass-ceramic was successfully synthesized by heat treatment of the precursor glass sample. XRD patterns of glass-ceramics samples were carried out to determine the precipitation of Na_3.6Y_1.8(PO₄)₃ crystals in the glass matrix. The effect of heat treatment time on the crystallinity and grain size of glass ceramics were discussed. The heat treatment temperature was 655℃ and the heat treatment time was 2 h. By comparing the up-conversion luminescence intensity of Ho³⁺ doped glass-ceramics with that of Ho³⁺-Yb³⁺ co-doped glass-ceramics, the optimum doping molar ratio of Ho³⁺ to Yb³⁺ was determined to be 1:2. At the same time, the energy transfer between Ho³⁺-Yb³⁺ was discussed. The up-conversion luminescence quantum efficiency of the samples were measured by integrating sphere.
- glass-ceramics,
- phosphate,
- Ho³⁺-Yb³⁺ co-doped,
- luminescence,
- quantum efficiency
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通讯作者: 陈斌, bchen63@163.com

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沈阳化工大学材料科学与工程学院沈阳 110142

Preparation and Luminescence Properties of Ho3+-Yb3+ Co-doped Phosphate Glass-Ceramics

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通讯作者: 陈斌, bchen63@163.com

Preparation and Luminescence Properties of Ho³⁺-Yb³⁺ Co-doped Phosphate Glass-Ceramics