Citation: RAO Yan-Ying, LI Zhang-Liang, HUANG Jian-Hui, JIANG Yu-Hang, ZHAO Xiao-Xu. Preparation and SERS Properties of 3D Ordered Gold Nanoshells Arrays[J]. Chinese Journal of Inorganic Chemistry, ;2018, 34(7): 1231-1239. doi: 10.11862/CJIC.2018.165 shu

Preparation and SERS Properties of 3D Ordered Gold Nanoshells Arrays

Fujian Provincial Key Laboratory of Ecology-Toxicological Effects & Control for Emerging Contaminants, Key Laboratory of Ecological Environment and Information Atlas, Fujian Provincial University, College of Environmental and Biological Engineering, Putian University, Putian, Fujian 351100, China

Corresponding author: RAO Yan-Ying, yanyingrao@ptu.edu.cn
Received Date: 15 February 2018
Revised Date: 19 April 2018

Figures(9)

The controllable preparation of three-dimensional ordered gold nano-shells (GNSs) structure was carried out by SiO₂ colloidal crystal as template and H₂O₂ as reducing agent in situ growth of gold seed, and then surface enhanced Raman spectroscopy (SERS) properties were studied in the growth process. The experimental results show that the controllable batch preparation of three-dimensional ordered GNSs array can be achieved by controlling the reaction time, reaction temperature, reducing agent H₂O₂ and the quantity of growth liquid K₂CO₃-HAuCl₄, and the hollow ordered GNSs structure is obtained by removing the SiO₂ core. Through the study of its SERS properties, it is found that the SiO₂ surface is completely covered by Au with rough structure showing the best SERS performance, and the corresponding hollow ordered GNSs structure shows superior SERS activity.
- gold nanoshells,
- gold nanomaterials,
- order arrays,
- porous materials,
- surface enhanced Raman spectroscopy
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