Citation: LUO Yi-Wei, PAN En-Ze, CHU Jing-Jing, YANG Jian-Hua, WANG Jin-Qu, HE Gao-Hong, LU Jin-Ming. Synthesis and Hydrothermal/Acid Stability of High Performance Zeolite T Membrane[J]. Chinese Journal of Inorganic Chemistry, ;2018, 34(7): 1351-1364. doi: 10.11862/CJIC.2018.156 shu

Synthesis and Hydrothermal/Acid Stability of High Performance Zeolite T Membrane

1.
State Key Laboratory of Fine Chemicals, Institute of Adsorption and Inorganic Membrane, School of Chemical Engineering, Dalian University of Technology, Dalian, Liaoning 116024, China
2.
State Key Laboratory of Fine Chemicals, School of Petroleum and Chemical Engineering, Dalian University of Technology, Panjin, Liaoning 124221, China

Corresponding author: YANG Jian-Hua, yjianhua@dlut.edu.cn
Received Date: 30 January 2018
Revised Date: 25 April 2018

Figures(10)

The influences of seed crystals and crystallization temperatures on the formation evolution and performance of zeolite T membranes were investigated, revealing that dense membranes could be obtained by using smaller seeds and the membrane growth rate was significantly affected by crystallization temperature. High performance zeolite T membranes with flux of 6.21 and 5.98 kg·m^-2·h^-1 respectively and high separation factor (> 10 000) for 90%(w/w) isopropanol solution at 348 K were obtained by using 0.4 and 0.6 μm seeds at 423 K for 4 h. A much long synthesis time was required at low temperature for achieving similar separation performance. It was found that the membrane formation was governed by the same mechanism of epitaxial growth, independent on the seed size and morphology and the crystallization temperature for the investigated synthesis solution. Furthermore, the zeolite T membranes show good hydrothermal and acid stability.
- zeolite T membrane,
- pervaporation,
- orientation,
- hydrothermal/acid stability
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