Citation: ZHOU Hui, LI Sha, XIAO Li-Ping, FAN Jie, ZHENG Xiao-Ming. Synthesis and Application of Super-Hydrophobic Titanosilicates Sphere[J]. Chinese Journal of Inorganic Chemistry, ;2018, 34(6): 1051-1058. doi: 10.11862/CJIC.2018.123 shu

Synthesis and Application of Super-Hydrophobic Titanosilicates Sphere

ZHOU Hui ^1,2,3 ,
LI Sha ⁴ ,
XIAO Li-Ping ^1,, ,
FAN Jie ¹ ,
ZHENG Xiao-Ming ¹

1.
Department of Chemistry, Zhejiang University, Hangzhou 310027, China
2.
College of Chemical and Biological Engineering, Zhejiang University, Hangzhou 310027, China
3.
Hangzhou First Applied Material Co., Ltd., Hangzhou 311300, China
4.
Key Laboratory of Chemical Utilization of Forestry Biomass of Zhejiang Province, Zhejiang A & F University, Hangzhou 311300, China

Corresponding author: XIAO Li-Ping, lpxiao@zju.edu.cn
Received Date: 15 December 2017
Revised Date: 23 March 2018

Figures(12)

Layered organo-titanosilicate materials with a micro sphere morphology (denoted as ms-LOTS) were synthesized via the aerosol-assisted self-assembly (AASA) method. The morphology and materials' structure of ms-LOTS was characterized by SEM, XRD and FT-IR. The temperature and concentration play an important role in catalytic activity. The ms-LOTS with a uniform sphere size of 2~4 μm were successfully prepared by the optimization of synthetic condition (350℃ and low concentration). At room temperature, ms-LOTS show improved catalytic performance in the epoxidation of cyclohexene.
- titanosilicate,
- super-hydrophobicity,
- organo-inorgano hybrid,
- micro sphere material
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