Advanced Search

Citation: ZHOU Xiang, WANG Xiu-Ling, LIU Yong-Jian, CHEN Yong-Bing, LIU Min. Preparation and Characterization of Fe3O4/PEI/Au@CdSe/CdS Multifunctional Composite Materials[J]. Chinese Journal of Inorganic Chemistry, ;2015, (6): 1165-1170. doi: 10.11862/CJIC.2015.150 shu

Preparation and Characterization of Fe3O4/PEI/Au@CdSe/CdS Multifunctional Composite Materials

  • 1.

    1 School of Chemistry Biology and Material Engineering, Suzhou University of Science and Technology, Suzhou, Jiangsu 215009, China;

  • 2.

    2 Key Laboratory of Environmental Functional Materials of Jiangsu Province, Suzhou, Jiangsu 215009, China

  • Corresponding author: LIU Yong-Jian, 
  • Received Date: 16 January 2015
    Available Online: 11 March 2015

    Fund Project: 国家自然科学基金(No.51103120)资助项目。 (No.51103120)

  • Fe3O4 nanoparticles were prepared by coprecipitation, which were modified by polyethyleneimine(PEI). Au nanoparticles were composited in situ, and then the Fe3O4/PEI/Au microspheres were obtained. CdSe/CdS QDs was modified with thioglycolic acid, and connected to magnetic nanoparticles. Fe3O4/PEI/Au@CdSe/CdS multifunctional composite microspheres were prepared successfully. Fourier transform infrared spectroscopy (FTIR), Fluorescence spectrophotometer, Fluorescence microscopy, X-ray diffraction (XRD), Transmission electron microscopy (TEM) and Vibrating sample magnetometer (VSM) are used for characterizing. The results shows that: the multifunctional composite microspheres with the size about 40 nm were superparamagnetic and remanence; the coercivity is near zero; the saturated magnetization is 28.83 A·m2·kg-1. What's more, the microspheres have both superior fluorescence and gold nanoparticles' properties.
  • 加载中
    1. [1]

      [1] Liang R P, Yao G H, Fan L X, et al. Anal. Chim. Acta, 2012,737:22-28

    2. [2]

      [2] Liu Q Y, Li H, Zhao Q R, et al. Mater. Sci. Eng., C, 2014, 41:142-151

    3. [3]

      [3] Gu L N, He X M, Wu Z Y. Mater. Res. Bull., 2014,59:65-68

    4. [4]

      [4] Sun H W, Zhu X J, Zhang L Y, et al. Mater. Sci. Eng., C, 2010,30:311-315

    5. [5]

      [5] Li Y C, Lin Y S, Tsai P J, et al. Anal Chem., 2007,79:7519-7525

    6. [6]

      [6] LIU Jing-Jing(刘静静), ZHANG Shu-Zheng(张书政), GONG Ke-Cheng(龚克成). Mater. Rev.(材料导报), 2003,17:78-81

    7. [7]

      [7] Liu Z G, Wang Y L, Zu Y G, et al. Mater. Sci. Eng., C, 2014, 42:31-37

    8. [8]

      [8] Demirci S, Sahiner N. J. Mol. Liq., 2014,194:85-92

    9. [9]

      [9] An F Q, Gao B J. J. Hazard. Mater., 2007,145:495-500

    10. [10]

      [10] Bao X L, Wang W, Wang C, et al. Biomater., 2014,35:8450-846

    11. [11]

      [11] Gao B J, Wang X P, Shen Y L. Biochem. Eng. J., 2006,28: 140-147

    12. [12]

      [12] Lokman N F, Bakar A A A, Suja F, et al. Sensor. Actuat., B: Chem., 2014,195:459-466

    13. [13]

      [13] Ohodnicki Jr P R, Brown T D, Holcomb G R, et al. Sens. Actuators B, 2014,202:489-499

    14. [14]

      [14] Nagata A, Oku T, Akiyama T, et al. Prog. Nat. Sci.: Mater. Int., 2014,24:179-183

    15. [15]

      [15] Choi J H, Kim H S, Choi J W, et al. Biosens. Bioelectron., 2013,49:415-419

    16. [16]

      [16] Wang H Y, Zhao B, Shen S S, et al. Vib. Spectrosc., 2014, 70:49-52

    17. [17]

      [17] Yang K, Huang K, He Z J, et al. Appl. Catal. B: Environ., 2014,158-159:250-257

    18. [18]

      [18] Tabakova T, Ilieva L, Petrova P, et al. Chem. Eng. J., 2015, 260:133-141

    19. [19]

      [19] He H, Lin Y X, Liu G Q, et al. Electrochem. Commun., 2014, 46:71-74

    20. [20]

      [20] Chang T L, Tsai C Y, Sun C C, et al. Microelectron. Eng., 2006,83:1630

    21. [21]

      [21] WU Wei(吴伟), HE Quan-Guo(贺全国), CHEN Hong(陈洪), et al. Acta Chim. Sinica(化学学报), 2007,65(13):1273-1279

    22. [22]

      [22] Yu H, Chen M, Rice P M, et al. Nano Lett., 2005,5(2):379-382

    23. [23]

      [23] Sun H W, Zhu X J, Zhang L Y, et al. Mater. Sci. Eng., C, 2010,30:311-315

    24. [24]

      [24] Vaneski A, Schneider J, Susha A S, et al. J. Photochem. Photobiol., C: Photochem. Rev., 2014,19:52-61

    25. [25]

      [25] CAO Y W, Banin U. J. Am. Chem. Soc., 2000,122(40):9692 -9702

    26. [26]

      [26] Bhargava R N, Gallagher D. Phys. Rev. Lett., 1994,72(3): 416-419

    27. [27]

      [27] WANG Xiu-Ling(王秀玲), GU Yin-Jun(顾银君), ZHUANG Hong(庒虹), et al. New Chem. Mater.(化工新型材料), 2012, 40(11):61-63

    28. [28]

      [28] Jana N R, Gearheart L, Murphy C J. J. Phys. Chem. B, 2001, 105:4065-4067

    29. [29]

      [29] GU Yin-Jun(顾银君), WANG Xiu-Ling(王秀玲), ZHAO Qin (赵勤), et al. Chem. J. Chinese Universities(高等学校化学 学报), 2012,5(33):885-891

    30. [30]

      [30] ZHANG Li-Jie(张利杰), GU Yin-Jun(顾银君), MA Qian(马 倩). J. Function. Mater.(功能材料), 2013:11(44):1588-1592

    31. [31]

      [31] HUANG Meng-Qiong(黄孟琼), WANG Xiu-Ling(王秀玲), LIU Yong-Jian(刘勇健). Acta Chim. Sinica(化学学报), 2010,68(16):1623-1628

  • 加载中
    1. [1]

      Zhaoyang WANG , Chun YANG , Yaoyao Song , Na HAN , Xiaomeng LIU , Qinglun WANG . Lanthanide(Ⅲ) complexes derived from 4′-(2-pyridyl)-2, 2′∶6′, 2″-terpyridine: Crystal structures, fluorescent and magnetic properties. Chinese Journal of Inorganic Chemistry, 2024, 40(8): 1442-1451. doi: 10.11862/CJIC.20240114

    2. [2]

      Xin XIONG , Qian CHEN , Quan XIE . First principles study of the photoelectric properties and magnetism of La and Yb doped AlN. Chinese Journal of Inorganic Chemistry, 2024, 40(8): 1519-1527. doi: 10.11862/CJIC.20240064

    3. [3]

      YanYuan Jia ,  Rong Rong ,  Jie Liu ,  Jing Guo ,  GuoYu Jiang ,  Shuo Guo . Unity is Strength, and Independence Shines: A Science Popularization Experiment on AIE and ACQ Effects. University Chemistry, 2024, 39(9): 349-358. doi: 10.12461/PKU.DXHX202402035

    4. [4]

      Qin Li ,  Kexin Yang ,  Qinglin Yang ,  Xiangjin Zhu ,  Xiaole Han ,  Tao Huang . Illuminating Chlorophyll: Innovative Chemistry Popularization Experiment. University Chemistry, 2024, 39(9): 359-368. doi: 10.3866/PKU.DXHX202309059

    5. [5]

      Siyi ZHONG , Xiaowen LIN , Jiaxin LIU , Ruyi WANG , Tao LIANG , Zhengfeng DENG , Ao ZHONG , Cuiping HAN . Targeting imaging and detection of ovarian cancer cells based on fluorescent magnetic carbon dots. Chinese Journal of Inorganic Chemistry, 2024, 40(8): 1483-1490. doi: 10.11862/CJIC.20240093

    6. [6]

      Shuwen SUN , Gaofeng WANG . Two cadmium coordination polymers constructed by varying Ⅴ-shaped co-ligands: Syntheses, structures, and fluorescence properties. Chinese Journal of Inorganic Chemistry, 2024, 40(3): 613-620. doi: 10.11862/CJIC.20230368

    7. [7]

      Ning LI , Siyu DU , Xueyi WANG , Hui YANG , Tao ZHOU , Zhimin GUAN , Peng FEI , Hongfang MA , Shang JIANG . Preparation and efficient catalysis for olefins epoxidation of a polyoxovanadate-based hybrid. Chinese Journal of Inorganic Chemistry, 2024, 40(4): 799-808. doi: 10.11862/CJIC.20230372

    8. [8]

      Yongming Guo ,  Jie Li ,  Chaoyong Liu . Green Improvement and Educational Design in the Synthesis and Characterization of Silver Nanoparticles. University Chemistry, 2024, 39(3): 258-265. doi: 10.3866/PKU.DXHX202309057

    9. [9]

      Siyu HOU , Weiyao LI , Jiadong LIU , Fei WANG , Wensi LIU , Jing YANG , Ying ZHANG . Preparation and catalytic performance of magnetic nano iron oxide by oxidation co-precipitation method. Chinese Journal of Inorganic Chemistry, 2024, 40(8): 1577-1582. doi: 10.11862/CJIC.20230469

    10. [10]

      Peiran ZHAO , Yuqian LIU , Cheng HE , Chunying DUAN . A functionalized Eu3+ metal-organic framework for selective fluorescent detection of pyrene. Chinese Journal of Inorganic Chemistry, 2024, 40(4): 713-724. doi: 10.11862/CJIC.20230355

    11. [11]

      Lina Liu ,  Xiaolan Wei ,  Jianqiang Hu . Exploration of Subject-Oriented Undergraduate Comprehensive Chemistry Experimental Teaching Based on the “STS Concept”: Taking the Experiment of Gold Nanoparticles as an Example. University Chemistry, 2024, 39(10): 337-343. doi: 10.12461/PKU.DXHX202405112

    12. [12]

      Yuanpei ZHANG , Jiahong WANG , Jinming HUANG , Zhi HU . Preparation of magnetic mesoporous carbon loaded nano zero-valent iron for removal of Cr(Ⅲ) organic complexes from high-salt wastewater. Chinese Journal of Inorganic Chemistry, 2024, 40(9): 1731-1742. doi: 10.11862/CJIC.20240077

    13. [13]

      Shengjuan Huo ,  Xiaoyan Zhang ,  Xiangheng Li ,  Xiangning Li ,  Tianfang Chen ,  Yuting Shen . Unveiling the Marvels of Titanium: Popularizing Multifunctional Colored Titanium Product Films. University Chemistry, 2024, 39(5): 184-192. doi: 10.3866/PKU.DXHX202310127

    14. [14]

      Peng XU , Shasha WANG , Nannan CHEN , Ao WANG , Dongmei YU . Preparation of three-layer magnetic composite Fe3O4@polyacrylic acid@ZiF-8 for efficient removal of malachite green in water. Chinese Journal of Inorganic Chemistry, 2024, 40(3): 544-554. doi: 10.11862/CJIC.20230239

    15. [15]

      Yonghui ZHOU , Rujun HUANG , Dongchao YAO , Aiwei ZHANG , Yuhang SUN , Zhujun CHEN , Baisong ZHU , Youxuan ZHENG . Synthesis and photoelectric properties of fluorescence materials with electron donor-acceptor structures based on quinoxaline and pyridinopyrazine, carbazole, and diphenylamine derivatives. Chinese Journal of Inorganic Chemistry, 2024, 40(4): 701-712. doi: 10.11862/CJIC.20230373

    16. [16]

      Yue Wu ,  Jun Li ,  Bo Zhang ,  Yan Yang ,  Haibo Li ,  Xian-Xi Zhang . Research on Kinetic and Thermodynamic Transformations of Organic-Inorganic Hybrid Materials for Fluorescent Anti-Counterfeiting Application information: Introducing a Comprehensive Chemistry Experiment. University Chemistry, 2024, 39(6): 390-399. doi: 10.3866/PKU.DXHX202403028

    17. [17]

      Yan ZHAO , Xiaokang JIANG , Zhonghui LI , Jiaxu WANG , Hengwei ZHOU , Hai GUO . Preparation and fluorescence properties of Eu3+-doped CaLaGaO4 red-emitting phosphors. Chinese Journal of Inorganic Chemistry, 2024, 40(10): 1861-1868. doi: 10.11862/CJIC.20240242

    18. [18]

      Xinyu Liu ,  Weiran Hu ,  Zhengkai Li ,  Wei Ji ,  Xiao Ni . Algin Lab: Surging Luminescent Sea. University Chemistry, 2024, 39(5): 396-404. doi: 10.3866/PKU.DXHX202312021

    19. [19]

      Ming ZHENG , Yixiao ZHANG , Jian YANG , Pengfei GUAN , Xiudong LI . Energy storage and photoluminescence properties of Sm3+-doped Ba0.85Ca0.15Ti0.90Zr0.10O3 lead-free multifunctional ferroelectric ceramics. Chinese Journal of Inorganic Chemistry, 2024, 40(4): 686-692. doi: 10.11862/CJIC.20230388

    20. [20]

      Nana Wang ,  Gaosheng Zhang ,  Huosheng Li ,  Tangfu Xiao . Discussion on the Teaching Reform of Environmental Functional Materials within the Context of “Double First-Class” Initiative: Emphasizing the Integration of Industry, Academia, Research, and Application. University Chemistry, 2024, 39(6): 137-144. doi: 10.3866/PKU.DXHX202312010

Get Citation
PDF
XML
Metrics
  • PDF Downloads(0)
  • Abstract views(503)
  • HTML views(32)

通讯作者: 陈斌, bchen63@163.com
  • 1. 

    沈阳化工大学材料科学与工程学院 沈阳 110142

  1. 本站搜索
  2. 百度学术搜索
  3. 万方数据库搜索
  4. CNKI搜索
Address：Zhongguancun North First Street 2,100190 Beijing, PR China Tel: +86-010-82449177-888
Powered By info@rhhz.net

/

DownLoad:  Full-Size Img  PowerPoint
Return