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Citation: WANG Li, ZHOU Yuan-Lin, LI Ying-Jun. Controlled Synthesis and Luminescence Properties of Ginkgo-Like PbWO4[J]. Chinese Journal of Inorganic Chemistry, ;2014, 30(4): 828-836. doi: 10.11862/CJIC.2014.099 shu

Controlled Synthesis and Luminescence Properties of Ginkgo-Like PbWO4

  • 1.

    1 State Key Laboratory Cultivation Base for Nonmetal Composites and Functional Materials, Southwest University of Science and Technology, Mianyang, Sichuan 621010, China;

  • Corresponding author: ZHOU Yuan-Lin, 
  • Received Date: 6 September 2013
    Available Online: 30 October 2013

    Fund Project: 国家自然科学基金委员会-中国工程物理研究院联合基金(No.11176026)资助项目。 (No.11176026)

  • In this paper, Ginkgo-like PbWO4 has been synthesized using direct precipitation method, taking sodium tartrate as the surfactant. The structure and property of synthesized products have been characterized by combination of scanning electron microscope (SEM), X-ray power diffraction (XRD), energy dispersive X-ray spectroscopy (EDS) and fluorescence emission spectra (PL). Investigations were carried out on the sodium tartrates inhibitory effect on the crystal face(004), and the impact of pHvalue and aging temperature on products morphology. Aprobable mechanism for products formation is proposed based on the internal crystal structure analysis. The results indicated that the most uniform crystal morphology will be obtained at the aging temperature of 30 ℃. PbWO4 crystal presented intense green emission under ultraviolet excitation, which will reach a maximum luminous intensity at pH=9.
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    1. [1]

      [1] Peng X G, Manna L, Yang W D, et al. Nature, 2000, 404:59-61

    2. [2]

      [2] El-Sayed M A. Acc. Chem. Res., 2001, 34, 257-264

    3. [3]

      [3] Zhou K B, Wang X, Sun X M, et al. Catal., 2005, 229:206-212

    4. [4]

      [4] Tang Z Y, Kotov N A. Adv. Mater., 2005, 17:951-962

    5. [5]

      [5] Schüth F. Angew Chem. Int. Ed., 2003, 42:3604-3622

    6. [6]

      [6] Qi L M, Clfen H, Antonietti M. Angew. Chem. Int. Ed. 2000, 39:604-606

    7. [7]

      [7] Yu S H, Antonietti M, Clfen H. Nano Lett., 2003, 3:379-382

    8. [8]

      [8] Lei F, Yan B, Chen H H, et al. Cryst. Growth Des., 2009, 9: 3730-3736

    9. [9]

      [9] Huo L, Chu Y. Mater. Lett., 2006, 60:2675-2681

    10. [10]

      [10] Annenkov A, Korzhik M, Lecoq P, et al. Nucl. Instrum. Methods Phys. Res. A, 2002, 490:30-50

    11. [11]

      [11] WANG Bu-Guo(王步国), SHI Er-Wei(施尔畏), ZHONG Wei-Zhuo(仲维卓), et al. Chinese J. Inorg. Mater.(无机材料 学报), 1998, 13(5):648-654

    12. [12]

      [12] Wang G Z, Hao C C, Zhang Y F. Mater. Lett., 2008, 62: 3163-3166

    13. [13]

      [13] Chen D, Shen G Z, Tang K B, et al. Phy. Chem. B, 2004, 108:11280-11284

    14. [14]

      [14] WANG Bing-Xi(王炳喜), ZUO Zheng-Hu(左正笏). Chinese J. Synth. Cryst.(人工晶体学报), 2008, 37:1295-1299

    15. [15]

      [15] Liu B, Yu S H, Li L J, et al. Angew. Chem. Int. Ed., 2004, 43:4745-4750

    16. [16]

      [16] George T, Joseph S, Sunny A, er al. Nanopaticle Res., 2008, 10:567-575

    17. [17]

      [17] ZHAO Shu-Li(赵书力), GUAN Ming-Yun(关明云), SUN Jian-Hua(孙建华), et al. Chinese J. Inorg. Chem.(无机化学 学报), 2011, 27(4):637-642

    18. [18]

      [18] Geng J, Lu D J, Zhu J J, et al. Phys. Chem. B, 2006, 110, 13777-13785

    19. [19]

      [19] Zhao W, Song X, Chen G, et al. Mater. Lett., 2009, 63:285-288

    20. [20]

      [20] WEI Xia(魏霞), ZHOU Yuan-Lin(周元林), LI Yin-Tao (李银涛), et al. Chinese J. Inorg. Chem.(无机化学学报), 2013, 29(3):583-588

    21. [21]

      [21] Geng J, Lü Y, Lu D, et al. Nanotechnology, 2006, 17:2614 -2620

    22. [22]

      [22] FENG Yi(冯怡), MA Tian-Ji(马天翼), LIU Lei(刘蕾), et al. Chinese J. Sci. in China Ser. B(中国科学:B), 2009, 39(9): 864-886

    23. [23]

      [23] Geng J, Zhu J J, Chen H Y. Cryst. Growth Des., 2006, 6: 321-326

    24. [24]

      [24] Yu J G, Zhao X F, Liu S W, et al. Appl. Phys. A, 2007, 87: 113-120

    25. [25]

      [25] YE Chong-Zhi(叶崇志), YANG Pei-Zhi(杨培志). Chinese J. Synth. Cryst.(人工晶体学报), 2005, 34:124-130

  • 加载中
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