Citation: FAN Ying-Hua, LUO Qin, LIU Gui-Xia, WANG Jin-Xian, DONG Xiang-Ting, YU Wen-Sheng, SUN De. Hydrothermal Synthesis and Photocatalysis of SnS₂ Nanomaterials[J]. Chinese Journal of Inorganic Chemistry, ;2014, 30(3): 627-632. doi: 10.11862/CJIC.2014.093 shu

Hydrothermal Synthesis and Photocatalysis of SnS₂ Nanomaterials

1.
1 Key Laboratory of Applied Chemistry and Nanotechnology at Universities of Jilin Province, Changchun University of Science and Technology, Changchun 130022, China;

Received Date: 26 August 2013
Available Online: 28 November 2013
Fund Project: 国家自然科学基金(NO.51072026) (NO.51072026)吉林省科技发展计划项目(NO.20130206002GX)资助项目。 (NO.20130206002GX)

SnS₂ nanomaterials with different morphologies were synthesized by hydrothermal method using different surfactants and different sulfur sources. The influence of reaction condition on morphology and property was discussed. The structure and composition of the as-prepared SnS₂ nanomaterials were characterized by X-ray diffraction (XRD), scanning electron microscope (SEM) and Brunauer-Emmett-Teller (BET) surface area analysis. The photocatalytic performance of the as-synthesized SnS₂ was evaluated by catalytic degradation of Rhodamine B (RhB). The results show that the surfactant and sulfur source play an important role in the structure and morphology of SnS₂. When the molar ratio of Sn⁴⁺ to Surfactant is 1:1, the samples are all pure hexagonal phase SnS₂. The obtained SnS₂ nanoplates employing sodium citrate as surfactant and thiourea as sulfur source show the best photocatalytic performance and the larger BET surface area.
- hydrothermal method;SnS₂;photocatalysis;nanomaterials
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沈阳化工大学材料科学与工程学院沈阳 110142

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Hydrothermal Synthesis and Photocatalysis of SnS₂ Nanomaterials