Citation: FAN Ying-Hua, LUO Qin, LIU Gui-Xia, WANG Jin-Xian, DONG Xiang-Ting, YU Wen-Sheng, SUN De. Hydrothermal Synthesis and Photocatalysis of SnS2 Nanomaterials[J]. Chinese Journal of Inorganic Chemistry, ;2014, 30(3): 627-632. doi: 10.11862/CJIC.2014.093
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SnS2 nanomaterials with different morphologies were synthesized by hydrothermal method using different surfactants and different sulfur sources. The influence of reaction condition on morphology and property was discussed. The structure and composition of the as-prepared SnS2 nanomaterials were characterized by X-ray diffraction (XRD), scanning electron microscope (SEM) and Brunauer-Emmett-Teller (BET) surface area analysis. The photocatalytic performance of the as-synthesized SnS2 was evaluated by catalytic degradation of Rhodamine B (RhB). The results show that the surfactant and sulfur source play an important role in the structure and morphology of SnS2. When the molar ratio of Sn4+ to Surfactant is 1:1, the samples are all pure hexagonal phase SnS2. The obtained SnS2 nanoplates employing sodium citrate as surfactant and thiourea as sulfur source show the best photocatalytic performance and the larger BET surface area.
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