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Citation: HU Zhi-Li, LI Chang-Sheng, TANG Hua, CHEN Lin, LIANG Jia-Qing, TANG Guo-Gang, ZHANG Yi. Preparation, Characterization and Tribological Properties of NbS2-xSex[J]. Chinese Journal of Inorganic Chemistry, ;2014, (2): 284-292. doi: 10.11862/CJIC.2014.024 shu

Preparation, Characterization and Tribological Properties of NbS2-xSex

  • 1.

    1 School of Mechanical Engineering, Jiangsu University, Zhenjiang, Jiangsu 212013, China;

  • Corresponding author: LI Chang-Sheng,  TANG Hua, 
  • Received Date: 20 May 2013
    Available Online: 11 July 2013

    Fund Project:

  • In this paper, NbS2-xSex nanoparticles were synthesized by solid state reaction. The effect of Se doped amount, reaction temperature and reaction time on evolution rules of crystal form and morphology of the production of Nb2-xSex nanomaterials were discussed, phase and microstructure of as-synthesized samples were examined by means of XRD, SEM, TEM and HRTEM. The results show that the morphology of NbS2-xSex nanobelt(nanoclintheriform) turned into nanoflake after Se was doped, meanwhile diffraction peaks were broadened, peak intensity become weaker, grains were refined. What's more, the doping amount, reaction temperature and reaction time play a greater impact on the morphology of the production. The morphology of NbS1.9Se0.1 which was doped by 5at% Se at 750 ℃ for 2h was fine. The results of UMT-2 tribology experiment show that the doped NbS2-xSex has excellent friction performance when NbS2-xSex was used as additive in liquid paraffin oil. Furthermore the NbS1.9Se0.1 that doped 5at% Se, at 750 ℃ for 2 h, has the best friction performance and the friction mechanism was also explained at the same time.
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    1. [1]

      [1] Tang H, Cao K S, Wu Q, et al. Cryst. Res. Technol., 2011, 46:195-200

    2. [2]

      [2] LI Chang-Sheng(李长生), HAO Mao-De(郝茂德), LIU Yan- Qing(刘艳清), et al. Acta Mater. Composit. Sin.(复合材料 学报), 2008,6(25):181-185

    3. [3]

      [3] LIU Yan-Qing(刘艳清), ZHANG Jing(张静), WU Yu-Han(吴 钰涵), et al. Chin. J. Tribol.(摩擦学学报), 2012,32(5):452- 457

    4. [4]

      [4] JIN Yue(晋跃), LI Chang-Sheng(李长生), WANG Mu-Ju(王 木菊), et al. Chin. J. Vacuum Sci. Technol.(真空科学与技 术学院), 2011,31(5):646-651

    5. [5]

      [5] CAO Ke-Sheng(曹可生), LI Chang-Sheng(李长生), LI Song- Tian(李松田), et al. Chinese J. Inorg. Chem.(无机化学学 报), 2011,27(11):2150-2156

    6. [6]

      [6] LI Wen-Jing(李文静), TANG Hua(唐华), LUO Cong(罗聪), et al. Chinese J. Inorg. Chem.(无机化学学报), 2012,28(8): 1587-1592

    7. [7]

      [7] Chhowalla M, Amaratunga G., Nature, 2000,407(14):164-167

    8. [8]

      [8] Homyonfer M, Mastai Y, Hershfinkel M, et al. J. Am. Chem. Soc., 1996,118(33):7804-7808

    9. [9]

      [9] Rothschild A, RCohen S, Tenne R. Appl Phys Lett, 1999,75 (25):4025-4027

    10. [10]

      [10] Rapoport L, Lvovsky M, Lapsker I, et al. Wear, 2001,249 (1):149-156

    11. [11]

      [11] WANG Hai-Dou(王海斗), XU Bin-Shi(徐滨士), LIU Jia-Jun (刘家浚). Micro-and Nanoscale Chalcogenide Solid Lubri- cants(微纳米硫系固体润滑剂). Beijing: Science Press, 2008:20-21

    12. [12]

      [12] Rothschild A, Sloan J, Tenne R. J. Am. Chem. Soc., 2000, 122:5169-5179

    13. [13]

      [13] Rapoport L, Bilik Y, Feldman Y, et al. Nature, 1997,387 (19):791-793

    14. [14]

      [14] Rapoport L, Feldman Y, Homyonfer M. Wear, 1999,225- 229:975-982

    15. [15]

      [15] Tenne R, Margulis L, Genut M, et al. Nature, 1992,360:444- 446

    16. [16]

      [16] Margulies L, Salitra G, Tenne R, et al. Nature, 1993,365: 113-117

    17. [17]

      [17] Tenne. R. Chemistry-A European Journal, 2002,8(23):5297- 5304

    18. [18]

      [18] Feldman Y, Wasserman E, Srolovitz D J, et al. Science, 1995,267:222-226

    19. [19]

      [19] Chen J, Li S L, Xu Q, et al. Chem. Commun., 2002,18:1722- 1723

    20. [20]

      [20] Feldman Y, Zak A, Popovitz-Biro R, et al. Solid State Sci., 2002,2:663-667

    21. [21]

      [21] Yi Y P, Zhao Y M, Chang Z. Mater. Chem. Phys., 2002,73: 327-329

    22. [22]

      [22] Lokhandea B J, Patila P S, Uplaneb M D. Physica B, 2001, 59:302-303

    23. [23]

      [23] Chen G H, Hou Z F, Gong X G, et al. J. Appl. Phys., 2008, 104(7):074101

    24. [24]

      [24] Xiong Y H, Tu H L, Du J, et al. Appl. Phys. Lett., 2010,97 (1):012901

    25. [25]

      [25] Frank S N, Bard A J. J. Am. Chem. Soc., 1977,99(14):4667- 4675

    26. [26]

      [26] Frank S N, Bard A J. J. Am. Chem. Soc., 1977,99(1):303-304

    27. [27]

      [27] Frank S N, Bard A J. J. Phys. Chem., 1997,81(15):1484-1489

    28. [28]

      [28] Akhtar J, Afzaal M, Banski M, et al. J. Am. Chem. Soc., 2011,133:5602-5609

    29. [29]

      [29] Wang J J, Xue D J, Guo Y G, et al. J. Am. Chem. Soc., 2011,133:18558-18561

    30. [30]

      [30] Sugawara K, Yokota K, Tanokura Y, et al. J. Low Temperat. Phys., 1993,90:305-317

    31. [31]

      [31] Onicha A C, Petchsang N, Kosel T H, et al. ACS Nano, 2012,6(3):2833-2843

    32. [32]

      [32] Xu J, Tang Y B, Chen X, et al. Adv. Funct. Mater., 2010, 20:4190-4195

    33. [33]

      [33] Wang M, Fei G T, Zhang Y G, et al. Adv. Mater., 2007,19: 4491-4494

    34. [34]

      [34] Boukhris N, Meradji H, Ghemid S, et al. Physica Scripta, 2011,83(06):065701-065709

    35. [35]

      [35] Curzon A E, Rajora O S. Phys. Stat. Sol.(a), 1988,105:335- 343

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