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Citation: HU Zhi-Li, LI Chang-Sheng, TANG Hua, CHEN Lin, LIANG Jia-Qing, TANG Guo-Gang, ZHANG Yi. Preparation, Characterization and Tribological Properties of NbS2-xSex[J]. Chinese Journal of Inorganic Chemistry, ;2014, (2): 284-292. doi: 10.11862/CJIC.2014.024 shu

Preparation, Characterization and Tribological Properties of NbS2-xSex

  • 1.

    1 School of Mechanical Engineering, Jiangsu University, Zhenjiang, Jiangsu 212013, China;

  • Corresponding author: LI Chang-Sheng,  TANG Hua, 
  • Received Date: 20 May 2013
    Available Online: 11 July 2013

    Fund Project:

  • In this paper, NbS2-xSex nanoparticles were synthesized by solid state reaction. The effect of Se doped amount, reaction temperature and reaction time on evolution rules of crystal form and morphology of the production of Nb2-xSex nanomaterials were discussed, phase and microstructure of as-synthesized samples were examined by means of XRD, SEM, TEM and HRTEM. The results show that the morphology of NbS2-xSex nanobelt(nanoclintheriform) turned into nanoflake after Se was doped, meanwhile diffraction peaks were broadened, peak intensity become weaker, grains were refined. What's more, the doping amount, reaction temperature and reaction time play a greater impact on the morphology of the production. The morphology of NbS1.9Se0.1 which was doped by 5at% Se at 750 ℃ for 2h was fine. The results of UMT-2 tribology experiment show that the doped NbS2-xSex has excellent friction performance when NbS2-xSex was used as additive in liquid paraffin oil. Furthermore the NbS1.9Se0.1 that doped 5at% Se, at 750 ℃ for 2 h, has the best friction performance and the friction mechanism was also explained at the same time.
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