Citation: CAI Wei-Wei, YANG Hui, GUO Xing-Zhong. Preparation, Characterization and Infrared Emissivity of ZnO Nanorod/Mica Composites[J]. Chinese Journal of Inorganic Chemistry, ;2014, (2): 229-234. doi: 10.11862/CJIC.2014.011 shu

Preparation, Characterization and Infrared Emissivity of ZnO Nanorod/Mica Composites

1.
Department of Materials Science and Engineering, Zhejiang University, Hangzhou 310027, China

Corresponding author: GUO Xing-Zhong,
Received Date: 17 June 2013
Available Online: 9 September 2013
Fund Project:

ZnO nanorod/Mica composite powders were successfully fabricated with chemical liquid deposition (CLD). The composite powder consisting of mica and ZnO nanorod was fabricated via a two-step process: (1) The ZnO colloid particles were absorbed on the surface of sheetlike mica particles via electrostatic interaction, and then heat-treatment was used to attain mica particles with ZnO nanocrystals loaded on the surface; (2) Precursor solution prepared with zinc sulfate heptahydrate, ethanolamine and ammonia was used to load ZnO nanorods on the surface of mica. The resultant composite particles were characterized by XRD, Zeta potential analyzer, scanning electron microscope (SEM) and spectral radiometer. The results showed that the ζ potential of mica in the ethanol/water solution (1:1, V/V) was -37 mV, while the ζ potential of ZnO colloidal particles was 16 mV. Thus the ZnO colloidal particles can be absorbed on the surface of mica particles via electrostatic interaction. As increased deposition density of ZnO nanorod on the surface of mica particles, the emissivity of the particles in 8~14 μm region increased from 0.800 to 0.863. Compared with the rodlike ZnO particles, the aggregation of structural unit had no obvious effect on the infrared emissivity of the particles.
- zinc oxide;mica;composite particles;infrared emissivity
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沈阳化工大学材料科学与工程学院沈阳 110142