Citation: Heyu Li, Lingjiao Li, Haiyu Wang, Bin Liu, Lianfen Chen, Zhiliang Jin. Chirality regulated CdS/Co-doped Ti₃C₂ MXene Schottky heterojunction for microplastic photoreforming to hydrogen and pyruvic acid[J]. Acta Physico-Chimica Sinica, ;2026, 42(10): 100350. shu

Chirality regulated CdS/Co-doped Ti₃C₂ MXene Schottky heterojunction for microplastic photoreforming to hydrogen and pyruvic acid

Heyu Li ¹ ,
Lingjiao Li ² ,
Haiyu Wang ^2,, ,
Bin Liu ³ ,
Lianfen Chen ⁴ ,
Zhiliang Jin ^1,,

1.
School of Chemistry and Chemical Engineering, Key Laboratory for Chemical Engineering and Technology, State Ethnic Affairs Commission, Ningxia Key Laboratory of Solar Chemical Conversion Technology, North Minzu University, Yinchuan 750021, Ningxia Hui Autonomous Region, China;
2.
School of Chemistry and Chemical Engineering, Yulin University, Yulin 719000, Shaanxi Province, China;
3.
School of Chemistry and Civil Engineering, Shaoguan University, Shaoguan 512005, Guangdong Province, China;
4.
School of Environmental and Chemical Engineering, Zhaoqing University, Zhaoqing 526061, Guangdong Province, China

Corresponding author: Haiyu Wang, Zhiliang Jin,
Received Date: 10 May 2026
Revised Date: 9 June 2026
Accepted Date: 16 June 2026

Chiral photocatalysts show significant promise for photocatalytic hydrogen evolution. However, chirality-regulated cadmium sulfide (CCdS) continues to suffer from insufficient photogenerated charge separation, which restricts its practical application and further advancement. Herein, we construct a novel Schottky heterojunction photocatalyst (CCdS/CTC) composed of CCdS and Co-doped Ti₃C₂ (CTC) via a simple physical mixing method. Notably, the photocatalyst achieves a hydrogen yield of 21937 μmol g^-1 from polylactic acid (PLA) microplastics within 5 h, accompanied by simultaneous conversion of PLA into pyruvic acid (PA) small molecules. X-ray photoelectron spectroscopy (XPS) and density functional theory (DFT) calculations demonstrate the interfacial charge transfer between CCdS and CTC upon contact, and in situ XPS confirms the charge transfer under illumination. Photoelectrochemical measurements demonstrate that the chirality regulation of CCdS works synergistically with the constructed heterojunction to effectively promote photogenerated charge separation and transport. The Schottky heterojunction formed at the CCdS/CTC interface further enhances the photogenerated carrier separation efficiency of CCdS. The synergy between chirality regulation and elemental doping markedly suppresses photogenerated charge recombination and optimizes surface reaction kinetics. This work presents a promising approach for converting plastic waste into H₂ fuel, offering critical insights into the rational design of sustainable photocatalysts for environmental remediation and renewable energy production.
- Chiral control,
- CdS,
- MXene,
- Schottky heterojunction,
- Microplastic hydrogen production
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通讯作者: 陈斌, bchen63@163.com

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沈阳化工大学材料科学与工程学院沈阳 110142

Chirality regulated CdS/Co-doped Ti3C2 MXene Schottky heterojunction for microplastic photoreforming to hydrogen and pyruvic acid

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通讯作者: 陈斌, bchen63@163.com

Chirality regulated CdS/Co-doped Ti₃C₂ MXene Schottky heterojunction for microplastic photoreforming to hydrogen and pyruvic acid