Citation: Qi Xun SHI, Rong Wen LU, Zhu Xia ZHANG, De Feng ZHAO. Preparation of Sulphur-containing Aromatic Amines by Reduction of the Corresponding Aromatic Nitro Compounds with Hydrazine Hydrate over Iron Oxide Hydroxide Catalyst[J]. Chinese Chemical Letters, ;2006, 17(8): 1045-1047. shu

Preparation of Sulphur-containing Aromatic Amines by Reduction of the Corresponding Aromatic Nitro Compounds with Hydrazine Hydrate over Iron Oxide Hydroxide Catalyst

State Key Laboratory of Fine Chemicals, Dalian University of Technology, Dalian 116012

Received Date: 13 February 2006

Sulphur-containing aromatic nitro compounds were rapidly reduced to the corresponding amines in high yields by employing hydrazine hydrate as a hydrogen donor in the presence of iron oxide hydroxide catalyst. It was worth noting that the catalyst exhibited extremely high activity. The reduction could be completed within 20-50 min and the yields were up to 97-99%.
- Iron oxide hydroxide catalyst,
- hydrazine hydrate,
- sulphur-containing aromatic nitro compounds,
- reduction
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