Citation: Wu Yan ZHANG, Ji Yu GUO, Xiao Tian LIANG. Studies on Agarofurans Ⅰ. New Synthesis of Nor-Ketoagarofuran and 4-Hydroxydihydroagarofuran[J]. Chinese Chemical Letters, ;1997, 8(1): 25-26. shu

Studies on Agarofurans Ⅰ. New Synthesis of Nor-Ketoagarofuran and 4-Hydroxydihydroagarofuran

Institute of Materia Medica, Chinese Academy of Medical Sciences & Peking Union Medical College, Beijing 100050

Received Date: 5 November 1996

Nor-ketoagarofuran (1),one of the furanoids isolated from agarowood oil,has been synthesized in a preparative scale in high yield from olefin 3 in 3 steps.Reaction of nor-ketoagarofuran (1) with CH₃MgI afforded 4-hydroxydihydroagarofuran (2),another naturally occurring tetrahydrofuran derivative.
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