Citation: Ping Yu DING, Xiao Xiang ZHU, Meng Shen CAI, De Quan YU. STUDIES ON THE TOTAL SYNTHESIS OF CIMICIFUGAMIDE FROM CIMICIFUGA DAHURICA[J]. Chinese Chemical Letters, ;1996, 7(6): 545-548. shu

STUDIES ON THE TOTAL SYNTHESIS OF CIMICIFUGAMIDE FROM CIMICIFUGA DAHURICA

a Department of organic Chemistry, School of pharmaceutical Sciences,Beijing Medical University, Beijing 100083;
b Institute of Materia Medica, Chinese Academy of Medical Sciences, Beijing 100050

Received Date: 30 November 1995

Cimicifugamide,a new natural compound isolated from the roots of Cimicifuga dahurica,was totally synthesized by a reaction sequence of seven steps in an overall yield of 31%.D-Galactose was used as starting material,trifluoroacetoxy was used as leaving group at C-1.The target product was characterized by IR,MS,¹H-NMR,¹³C-NMR and elemental analysis.
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