Citation: Jian Hua YU, Yu Lai HU, Shi Yan YANG, Yuan Qi YIN, Li Ping CAI. A Novel Condensation Reaction of Alkyl Aryl Ketone with Ethyl Ortho-Formate under Microwave Irradiation[J]. Chinese Chemical Letters, ;1998, 9(1): 1-4.
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Under microwave irradiation, boron trifluoride has been found to mediate a novel condensation reaction of alkyl aryl ketone with ethyl ortho-formate to give a series of new condensa-tion products (5,6,7,8). Their structures were determined by IR, 1H-/13C-NMR, MS spectra, and the crystal structure of 8 was further defined by X-ray diffraction.
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Keywords:
- microwave,
- irradiation,
- condensation,
- alkyl aryl ketone
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