Citation: Xin LIU, Rut Lian SHAO, Run Qiu HUANG. An Efficient Method for the Synthesis of Aliphatic α-Organothio Aldoximes[J]. Chinese Chemical Letters, ;1999, 10(2): 97-98.
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A new and simple procedure for the synthesis of aliphatic α-organothio aldoximes was reported. The aliphatic aldoxime was chlorinated by t-BuOCl, the resulting hydroxime acid chloride was treated with triethylamine and alkyl mercaptan in a one pot procedure to get the target compounds. The method is very efficient with high yield and good purity.
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