Citation: Xiao Kun HU, Ren Ao GU, Zhang Fei HE, Ke Qian CHEN, Da Qing SUN. DETECTION OF INTERMEDIATES IN REACTION BETWEEN N, N'-DI (P-METHYL) PHENYL MONOTHIOXAMIDES AND 1, 3-DIAMINE TRIMETHYLENE USING RAMAN SPECTROSCOPY[J]. Chinese Chemical Letters, ;1992, 3(7): 533-534. shu

DETECTION OF INTERMEDIATES IN REACTION BETWEEN N, N'-DI (P-METHYL) PHENYL MONOTHIOXAMIDES AND 1, 3-DIAMINE TRIMETHYLENE USING RAMAN SPECTROSCOPY

Xiao Kun HU ^a ,
Ren Ao GU ^a,b ,
Zhang Fei HE ^a,b ,
Ke Qian CHEN ^a,b ,
Da Qing SUN ^a,b

a The Central Lab. of Suzhou University, Suzhou, Jiangsu 215006;
b Chemistry Department of Suzhou University, Suzhou, Jiangsu 215006

Received Date: 29 February 1992

Reman spectroscopy is used as a tool to monitor the reaction between N,N'-di (pmethyl) monothioxamides and 1,3-diamine trimethylene and to detect the reaction intermediate. By observing changes of 1024 cm^-1 C=S band and appearance of a new bend at around 1720 cm^-1, the reaction mechanism is discussed.
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