Citation: Xi Liang GUO, Shao Min SHUANG, Jian Bin CHAO, Du Xin LI. Comparative Study on the Inclusion Interaction between meso-Tetrakis (4-N-ethylpyridiniurmyl) porphyrin and β-Cyclodextrin Derivatives[J]. Chinese Chemical Letters, ;2004, 15(8): 961-964. shu

Comparative Study on the Inclusion Interaction between meso-Tetrakis (4-N-ethylpyridiniurmyl) porphyrin and β-Cyclodextrin Derivatives

Institute of Advanced Chemistry, School of Chemistry and Chemical Engineering, Shanxi University, Taiyuan 030006

Received Date: 16 July 2003

Fund Project: This work was supported by the National Natural Science Foundation of China (No.20172035) and the National Education Committee Foundation for the Outstanding Younger Teachers and the Foundation of Shanxi Province.

The interaction of β-cyclodextrin (β-CD) and the modified cyclodextrins, hydroxy propyl-(-cyclodextrin (HP-β-CD), sulfobutylether-β-cyclodextrin (SBE-β-CD) and synthesized meso-tetrakis(4-N-ethylpyridiniurmyl)porphyrin (TEPyP) in aqueous solution has been studied by spectroscopic methods systematically.A significant change in fluorescence and absorption properties has been observed in the presence of β-CD, HP-β-CD and SBE-β-CD.The stoichiometry and formation constants have been determined by the steady-state fluorescence technique.The results showed that the β-CD derivatives were prior to the native β-CD and the hydrogen bonding and static electric forces played important roles in the formation of the inclusion complexes.The conformation was further confirmed by NMR spectroscopy.
- meso-Tetrakis (4-N-ethylpyridiniurmyl) porphyrin (TEPyP),
- cyclodextrin,
- absorption,
- fluorescence,
- nuclear magnetic resonance (NMR)
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