Citation: Da Yong SUN, Zi Yang LIU, Xing Hua GUO, Yi Min SHE, Yu ZHOU, Shu Ying LIU. A NEW METHOD FOR THE PREPARATION OF FULLEROL[J]. Chinese Chemical Letters, ;1996, 7(5): 431-432. shu

A NEW METHOD FOR THE PREPARATION OF FULLEROL

The Key Laboratory of Applied Spectroscopy, Changchun Institute of Applied Chemistry, Chinese Academy of Sciences, Changchun . Jilin 130022

Received Date: 3 November 1995

Fund Project: The authors thank the National Natural Science Foundation of China, the Yanbian Aodong Pharmaceuticals Ltd. and the Changchun Applied Chemistry Center for financial supports.

Reaction of C₆₀with excessive potassium in toluene at refluxing temperature results in black precipitate K₂C₆₀with high conversion,which can completely be hydrolyzed to prepare the fullerol.Investigations including FT-IR.¹H NMR.¹³C NMR.UV-Vis and FABMS of the product were reponed.
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