Citation: Wu-Yang Nie, Le Li, De-Liang Li, Xi Liu. A new preparation method of gold nanoparticles by intra-reduction of sodium gold(I) sulfite[J]. Chinese Chemical Letters, ;2014, 25(2): 380-382. shu

A new preparation method of gold nanoparticles by intra-reduction of sodium gold(I) sulfite

Wu-Yang Nie ^a ,
Le Li ^b ,
De-Liang Li ^a,, ,
Xi Liu ^a

1.
a Central South University of Forest and Technology, Changsha 410004, China;
2.
b University of Florida, 2800 SW Williston Road, Gainesville city, FL 32608, USA

Corresponding author: De-Liang Li,
Received Date: 22 September 2013
Available Online: 12 November 2013
Fund Project: This work was financially supported by the National Natural Science Foundation of China (No. 20976201) (No. 20976201)

In this study, well-dispersed gold nanoparticles were prepared by using intra-molecular reduction of sodium gold sulfite, without using additional reductants and chloride free. The technical parameters including transformation temperature, pH, and concentration were optimized by the single-factor method as 90 ℃, pH 1, and 0.01 mmol/L [Na₃Au(SO₃)₂], respectively. The resultant colloidal transmission electron microscopy images (TEM) and UV-vis absorption spectrophotometer spectra were acquired to check their properties, and the results show this kind of colloidal gold is controlled to 6 nm in sizes and has good stability in solution.
- Colloidal gold,
- Sodium gold(I) sulfite,
- Intra-reduction
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沈阳化工大学材料科学与工程学院沈阳 110142