Citation: ZHANG Yujing, DAI Xingchao, WANG Hongli, SHI Feng. Catalytic Synthesis of Formamides with Carbon Dioxide and Amines[J]. Acta Physico-Chimica Sinica, ;2018, 34(8): 845-857. doi: 10.3866/PKU.WHXB201701081 shu

Catalytic Synthesis of Formamides with Carbon Dioxide and Amines

ZHANG Yujing ^1,2 ,
DAI Xingchao ^1,2 ,
WANG Hongli ¹ ,
SHI Feng ^1,,

1.
State Key Laboratory for Oxo Synthesis and Selective Oxidation, Center for Green Chemistry and Catalysis, Lanzhou Institute of Chemical Physics, Chinese Academy of Sciences, Lanzhou 730000, P. R. China
2.
University of Chinese Academy of Sciences, Beijing 100049, P. R. China

Author Bio:

SHI Feng completed his Ph.D. studies in catalysis at LICP, CAS in 2004. After a three-year postdoctoral research in LIKAT in Germany, he joined the faculty of LICP in 2008 as Hundred Talents Program of CAS. Since 2016 SHI Feng is the deputy director of the State Key Laboratory for Oxo Synthesis and Selective Oxidation. His research focuses on nano-catalysis in fine chemical synthesis and C₁ chemistry
Corresponding author: SHI Feng, fshi@licp.cas.cn
Received Date: 30 November 2017
Revised Date: 29 December 2017
Accepted Date: 29 December 2017
Available Online: 8 August 2018
Fund Project: the National Natural Science Foundation of China 91745106the National Natural Science Foundation of China 21633013The project was supported by the National Natural Science Foundation of China (21633013, 91745106) and National Key Research and Development Program of China (2017YFA0403103)National Key Research and Development Program of China 2017YFA0403103

Carbon dioxide is a green C₁ resource that can be efficiently recycled by catalytic transformation into value-added chemicals. Formamides are important intermediates and solvents that are used extensively in pharmaceutical, daily-chemical, and petrochemical industry. Therefore, it is worthwhile to synthesize formamides with CO₂ and amines. In this review, the main advancements in the synthesis of formamides by using CO₂ as the C₁ feedstock with noble metal catalysts (Ir, Pd, Pt, Ru, Rh, etc.), non-noble metal catalysts (Ni, Mo, Cu, Fe, Co, Zn, Al, etc.), organocatalysts, and catalyst-free systems have been summarized. In addition, the role of the reducing agents such as H₂, silanes, and boranes involved in these transformations has also been reviewed. In addition, the reaction mechanisms with the different catalyst systems have been discussed.
- Carbon dioxide,
- Amines,
- Formamides,
- Carbonylation
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沈阳化工大学材料科学与工程学院沈阳 110142