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Citation: MA Juan, SONG Feng-Dan, ZHOU Ze-Qi, QI Sui-Tao, YI Chun-Hai, YANG Bo-Lun. Preparation and Optimization of Vertically Arrayed Zinc Oxide Nanorods[J]. Acta Physico-Chimica Sinica, ;2015, 31(11): 2213-2219. doi: 10.3866/PKU.WHXB201509301 shu

Preparation and Optimization of Vertically Arrayed Zinc Oxide Nanorods

1.
1 School of Chemistry Engineering and Technology, Xi'an Jiaotong University, Xi'an 710049, P. R. China;
2.
2 School of Chemical Engineering, Tianjin University, Tianjin 300072, P. R. China

Corresponding author: QI Sui-Tao,
Received Date: 11 June 2015
Available Online: 29 September 2015
Fund Project: 陕西省自然科学基金研究计划(2015JZ004)重点项目和多相流国家重点实验室课题项目资助 (2015JZ004)

A two-step method for growing vertical zinc oxide nanorod arrays on indium tin oxide (ITO)-coated glass substrates is proposed. First, a zinc oxide seed layer was formed on the ITO substrate by simple dipcoating combined with the Czochralski method, and then vertical zinc oxide nanorod arrays were obtained by a hydrothermal method. The nanorod arrays were characterized using X-ray diffraction (XRD), scanning electron microscopy (SEM) and energydispersive X-ray spectroscopy (EDS). The effects of the precursor concentration, sol-aging time, hydrothermal reaction time, and cycle times of the dip-coating and hydrothermal reaction on the structure and surface morphology of the zinc oxide nanorod arrays were investigated. The results show that the length and diameter of zinc oxide nanorod arrays increased with the increasing precursor concentrations, sol-aging time, and hydrothermal reaction time. Good vertical zinc oxide nanorod arrays were obtained under the optional growth conditions, i.e., three hydrothermal reactions for 150 min, three rounds of dip-coating, 0.5 mol·L^-1 precursor solution concentration, and 24 h aging.
- Zinc oxide nanorod array,
- Dip-coating and czochralski,
- Hydrothermal reaction,
- Aging time,
- Orientation
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