Citation: GUI Ming-Sheng, WANG Peng-Fei, YUAN Dong, TANG Miao-Miao. Preparation and Visible Light Photocatalytic Activity of 3D-NiO/Bi_7.47Ni_0.53O_11.73 Photocatalysts[J]. Acta Physico-Chimica Sinica, ;2013, 29(12): 2608-2614. doi: 10.3866/PKU.WHXB201310312 shu

Preparation and Visible Light Photocatalytic Activity of 3D-NiO/Bi_7.47Ni_0.53O_11.73 Photocatalysts

1.
College of Materials and Chemical Engineering, Sichuan University of Science & Engineering, Zi ng 643000, Sichuan Province, P. R. China

Received Date: 13 September 2013
Available Online: 31 October 2013
Fund Project: 四川省教育厅项目(13ZB0137) (13ZB0137) 四川理工学院人才引进项目(2012RC05) (2012RC05)

Three-dimensional (3D)-NiO/Bi_7.47Ni_0.53O_11.73 (BiNiO) microspheres were synthesized by a mixed solvothermal process in the presence of urea. The catalysts were characterized using X-ray diffraction (XRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM), X-ray photoelectron spectroscopy (XPS), ultraviolet-visible diffuse reflectance spectroscopy (UV-Vis DRS), and photodegradation of methyl orange (MO). The results show that the composite catalysts are composed of NiO nanosheets and 3D-NiO/Bi_7.47Ni_0.53O_11.73 microspheres. The sample BiNiO-300, which was prepared by heating the precursor at 300 ℃ for 2 h, had the best photocatalytic activity: after visible-light irradiation for 3 h, the decolorization of an MO solution was 98%.
- Composite,
- Photocatalytic,
- Visible light,
- Methyl orange
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通讯作者: 陈斌, bchen63@163.com

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沈阳化工大学材料科学与工程学院沈阳 110142

Preparation and Visible Light Photocatalytic Activity of 3D-NiO/Bi7.47Ni0.53O11.73 Photocatalysts

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通讯作者: 陈斌, bchen63@163.com

Preparation and Visible Light Photocatalytic Activity of 3D-NiO/Bi_7.47Ni_0.53O_11.73 Photocatalysts