Citation: CHEN Yang, WANG Cheng-Guo, ZHAO Wei. Fabrication of a Self-Healing Pure SiC Coating by a Two-Step Technique[J]. Acta Physico-Chimica Sinica, ;2012, 28(01): 239-244. doi: 10.3866/PKU.WHXB201228239 shu

Fabrication of a Self-Healing Pure SiC Coating by a Two-Step Technique

1.
1. Key Laboratory for Liquid-Solid Structural Evolution and Processing of Materials Ministry of Education, Shandong University, Jinan 250061, P. R. China;
2. Carbon Fiber Engineering Research Center, Shandong University, Jinan 250061, P. R. China

Received Date: 18 July 2011
Available Online: 28 October 2011
Fund Project: 国家重点基础研究发展规划项目(973) (2011CB605601) (973) (2011CB605601)国际科技合作项目(2009DFR50600)资助 (2009DFR50600)

A self-healing pure SiC coating was prepared on a carbon/carbon (C/C) composite by a two-step technique to protect the C/C composite from oxidation. First, SiC nanowires were obtained on the substrate surface by the thermal decomposition of hydrogen silicone oil (H-PSO). Second, a coating with a thickness of 100-200 μm was produced by infiltrating with silicon at high temperature in an ar n atmosphere. The morphology and phase composition of the coating were observed by X-ray diffraction (XRD) and scanning electron microscopy (SEM). Oxidation tests were carried out on specimens and the results indicated that the obtained coating consisted of pure SiC and had a certain self-healing ability. The SiC self-healing coating significantly increased the antioxidant properties of the C/C composites and it protected the C/C composites from oxidation at 1400 °C in air over 4 h with a corresponding mass loss of only 0.71%.
- C/C composite,
- SiC nanowire,
- SiC coating,
- Oxidation resistance,
- Self-healing
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