Citation: SUN Feng-Juan, WANG Jia. Development and Application of Virtual Potentiostat on Electrochemical Corrosion Measurement[J]. Acta Physico-Chimica Sinica, ;2012, 28(03): 615-622. doi: 10.3866/PKU.WHXB201201101 shu

Development and Application of Virtual Potentiostat on Electrochemical Corrosion Measurement

SUN Feng-Juan ,
WANG Jia

1.
College of Chemistry and Chemical Engineering, Ocean University of China, Qingdao 266100, Shandong Province, P. R. China; State Key Laboratory for Corrosion and Protection of Metals, Shenyang 110015, P. R. China

Received Date: 19 October 2011
Available Online: 10 January 2012
Fund Project: 国家自然科学基金(50971118, 51131005)资助项目 (50971118, 51131005)

A potentiostat is a fundamental piece of equipment for the study of corrosion electrochemistry and research into the application of virtual technology to potentiostats is becoming increasingly important. The functions of virtual potentiostats can be controlled and implemented using software instead of complex hardware. They would be capable of not only meeting the demands of a variety of electrochemical tests, but would also be more flexible offering a simpler structure and operating parameters. This would represent a significant development in virtual electrochemical corrosion instrumentation. In this paper, a virtual potentiostat measurement system VEC11-A (virtual electrochemical corrosion test system) has been designed based on LabVIEW. The virtual instrument system of the potentiostat, based on the proportionintegration- differentiation (PID) control technology operated under the LabVIEW 2010 programming platform, was used to determine corrosion potential measurement, polarization curves, linear polarization curves, cyclic voltammetry curves, dynamic potential anode passivation curves, and constant potential step curves. In contrast with normal electrochemical instruments, the system worked well for electrolyzers of different impedances.
- Virtual instrument,
- Steady-state polarization curve,
- Potentiostat,
- PID control,
- LabVIEW
1. [1]
  (1) Yang, L. P.; Li, H. T.; Xiao, K.; Yang, L. An Introduction to the Virtual Instrument Technology; Publishing House of Electronics industry: Beijing, 2003; pp 2-6. [杨乐平, 李海涛, 肖凯, 杨磊. 虚拟仪器技术概论, 北京: 电子工业出版社, 2003: 2-6.]
2. [2]
  (2) Li, Q. X.; Ren, Y. X. Modern Scientific Instruments 1999, 4, 10. [李青霞, 任焱晞. 现代科学仪器, 1999, 4, 10.]
3. [3]
  (3) Hu, G.; Zhang, S. T. Computers and Applied Chemistry 2006, 23 (5), 465. [胡舸, 张胜涛. 计算机与应用化学, 2006, 23 (5), 465.]
4. [4]
  (4) Pan, G. Y.;Wang, J. Journal of Chinese Society for Corrosion and Protection 2008, 28 (4), 210. [潘国运, 王佳. 中国腐蚀与防护学报, 2008, 28 (4), 210.]
5. [5]
  (5) Li, H. Q.; Luo, X. B.; Liu, C. X.; Jiang, L. Y.; Cui, D. F.; Cai, X. X. Multi-Channel Electrochemical Detection System Base on LabVIEW. In Information Acquisition, 2004 International Conference on Information Acquisition, Hefei,China, June 21-25, 2004; Yang, Q. D. Ed.; Press of University of Science and Technology of China: Hefei, 2005; pp 224-227.
6. [6]
  (6) Perusse, P.; Leech, D. Instrumentation Science & Technology 2000, 28 (1), 59.
7. [7]
  (7) Economou, A.; Bolis, S. D.; Efstathoou, C. E.; Volikakis, G. J. Analytica Chimica Acta 2004, 467, 179.
8. [8]
  (8) Han, L.; Mai,W.;Wang, S. Y.; Song, S. Z. Corrosion Science and Protection Technology 2004, 16 (1), 50. [韩磊, 买巍, 王守琰, 宋诗哲. 腐蚀科学与防护技术, 2004, 16 (1), 50.]
9. [9]
  (9) Han, L.; Song, S. Z. Journal of Chemical Industry and Engineering 2008, 59 (4), 977. [韩磊, 宋诗哲. 化工学报, 2008, 59 (4), 977.]
10. [10]
  (10) Zhong, H. J.; Deng, S. H. Analytical Instrumentation 2009, 2, 1. [钟海军, 邓少华. 分析仪器, 2009, 2, 1.]
11. [11]
  (11) Song, S. Z. Corrosion Electrochemical Research Methods; Chemical Industry Press: Beijing, 1988; pp 28-29. [宋诗哲. 腐蚀电化学研究方法. 北京: 化学工业出版社, 1988: 28-29.]
12. [12]
  (12) Jin, Q.; Deng, Z. J. Journal of Chongqing Institute of Technology 2008, 22 (5), 91. [金奇, 邓志杰. 重庆工学院学报, 2008, 22 (5), 91.]
13. [13]
  (13) Jin, Z. Q.; Bao, Q. L. Microcomputer Information 2005, 21 (6), 1. [金志强, 包启亮. 微计算机信息, 2005, 21 (6), 1.]
14. [14]
  (14) Jiang,W.; Yuan, F. Journal of East China Institute of Technology 2004, 12 (4), 395. [江伟, 袁芳. 东华理工学院学报, 2004, 12 (4), 395.]
15. [15]
  (15) Wang,W.; Zhang, J. T. Acta Automatica Sinica 2000, 26 (3), 348. [王伟, 张晶涛. 自动化学报, 2000, 26 (3), 348.]
16. [16]
  (16) Ruan, Q. Z. LabVIEW and Me —The Ten-year-programming Experience of a Engineer in NI; Beihang University Press: Beijing, 2009; pp 197-246. [阮奇桢. 我和LabVIEW—— 一个NI工程师的十年编程经验. 北京: 北京航空航天大学出版社, 2009: 197-246.]
17. [17]
  (17) Zhang, K.; Zhou, Z.; Guo, D. LabVIEW Virtual Instrument Engineering Design and Development; National Defence Industry Press: Beijing, 2004; pp 2-6. [张凯, 周陬, 郭栋. LabVIEW虚拟仪器工程设计与开发. 北京: 国防工业出版社, 2004: 2-6.]
18. [18]
  (18) Ye, X. S.; Zhang, G. D.; Gao, B.;Wang, P. Chinese Journal of Scientific Instrument 2005, 26 (10), 1002. [叶学松, 张贵东, 高波, 王平. 仪器仪表学报, 2005, 26 (10), 1002.]
19. [19]
  (19) Dai, F. P.; Lv, S. Y.; Feng, B. X.; Li, Q. Journal of Lanzhou University 2002, 38 (6), 44. [代富平, 吕淑媛, 冯博学, 李强. 兰州大学学报, 2002, 38 (6), 44.]
20. [20]
  (20) Fan, Z. X.; He,W.; Huo, C. H. Modern Scientific Instruments 2005, (3), 33. [范中晓, 何为, 霍彩虹. 现代科学仪器, 2005, (3), 33.]
21. [21]
  (21) Liu, Y. H. Electrochemical Measurement Technology; Beijing Aviation Institute Press: Beijing, 1987; pp 17-98. [刘永辉. 电化学测试技术. 北京: 北京航空学院出版社, 1987: 17-98.]
22. [22]
  (22) Wei, B. M. Metal Corrosion Theory and Application; Chemical Industry Press: Beijing, 1984; pp 170-221. [魏宝明. 金属腐蚀理论及应用. 北京: 化学工业出版社, 1984: 170-221.]
23. [23]
  (23) Zou, Y.;Wang, J. Acta Phys. -Chim. Sin. 2010, 26, 2361. [邹妍, 王佳. 物理化学学报, 2010, 26, 2361.]
24. [24]
  (24) Fan, X. Z.; Lu, Y. H.; Kong, X. F.; Xu, H. B.;Wang, J. Acta Phys. -Chim. Sin. 2011, 27, 887. [范新庄, 芦永红, 孔祥峰, 徐海波, 王佳. 物理化学学报, 2011, 27, 887.]
25. [25]
  (25) Wang, X. Y.;Wu, Y. X.; Zhang, L.; Yu, Z. Y. Corrosion Science and Protection Technology 2000, 12 (6), 311. [汪轩义, 吴荫顺, 张琳, 于正阳. 腐蚀科学与防护技术, 2000, 12 (6), 311.]
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