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Citation: ZHAO Hai-Jun, HOU Hai-Tao, CAO Jie-Ming ZHENG Ming-Bo, LIU Jing-Song, ZHANG Fang, . Solvothermal Synthesis of Mesoporous SnO₂ with Spongy Structure[J]. Acta Physico-Chimica Sinica, ;2007, 23(06): 959-963. doi: 10.3866/PKU.WHXB20070633 shu

Solvothermal Synthesis of Mesoporous SnO₂ with Spongy Structure

1.

Nanomaterials Research Institute, College of Materials Science and Technology, Nanjing University of Aeronautics and Astronautics, Nanjing 210016, P. R. China

Corresponding author: ,
Received Date: 31 October 2006
Available Online: 21 April 2007

Mesoporous tin dioxide (SnO2) was synthesized by thermal decomposition of the precursor obtained via a solvothermal method in the presence of SnCl4·5H2O, urea and ethanol. The calcined sample was characterized in detail by X-ray diffraction (XRD), Fourier transform infrared (FT-IR) techniques, transmission electron microscopy(TEM), thermal analysis (TG-DTA) and nitrogen adsorption-desorption measurements. The characterization results showed that the calcined sample in 300 ℃ was spongy structure tin dioxide with meso-porosity which was formed by accumulating nanoparticles (particle size: ca 5 nm). The pore size ranged from 2 to 8 nm, and the BET surface area increased to 134 m2·g-1.
- Tin dioxide; Solvothermal synthesis; Mesoporous; Nanoparticle; Heat treatment
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Solvothermal Synthesis of Mesoporous SnO2 with Spongy Structure

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通讯作者: 陈斌, bchen63@163.com

Solvothermal Synthesis of Mesoporous SnO₂ with Spongy Structure