Citation:
Cheng Hu-Min, Ma Yu-Rong, Liao Fu-Hui, Ma Ji-Ming, Qi Li-Min. Synthesis of Mesoporous Zirconia with Hydrothermal Homogeneous Precipitation Method[J]. Acta Physico-Chimica Sinica,
;2003, 19(04): 326-328.
doi:
10.3866/PKU.WHXB20030409
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Using urea as homogeneous precipitant, the precursor of mesoporous zirconia was synthesized by hydrothermal method. After heat-treatment at 500~550 ℃ for 2 h, the crystalline (t or m phase) mesoporous zirconia with short-range order was prepared. Their BJH desorption pore size and BET surface area are about 4~6 nm and 60~90 m2•g-1, respectively.
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