Citation: Li Gao-Ren, Tong Ye-Xiang, Liu Guan-Kun, Xu Chang-Wei. Electrochemical Preparation of Er-Ni-Co Alloy Film in DMSO[J]. Acta Physico-Chimica Sinica, ;2002, 18(08): 764-768. doi: 10.3866/PKU.WHXB20020819
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The cyclic voltammetry and potentiostatic electrolysis were used to investigate the preparation of Er-Ni-Co alloy films in LiClO4-DMSO system. Experimental results indicate that Er-Ni-Co alloy films containing Er from 9.21% to 18.90% were prepared from 0.1 mol•L-1 ErCl3-0.1 mol•L-1 NiCl2- 0.1 mol•L-1 CoCl2-0.1 mol•L-1LiClO4-DMSO system by potentiostatic electrolysis on Cu substrates at deposition potential from -2.20~-2.50 V (vs SCE). Their surfaces are black, uniform, adhesive, and have metallic luster.
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