Home

Citation: Wang Cun-Xin, Song Zhao-Hua, Xiong Wen-Gao, Qu Song-Sheng. Development of an Isperibel Reaction Calorimeter[J]. Acta Physico-Chimica Sinica, ;1991, 7(05): 586-588. doi: 10.3866/PKU.WHXB19910514 shu

Development of an Isperibel Reaction Calorimeter

1.
Chemistry Department, Wuhan University, Wuhan 430072

Received Date: 12 March 1990
Available Online: 15 October 1991

An isoperibel calorimeter for measnring heat of solid-liquid, liquid-liquid reactions was developed. Rection vessel made by resisting hard glass, its volume is about 100 cm~3, The precisions of cotrolling and measuring the tempreture were±0.001 K and ±0.0001 K respectively. The measnring error was 0.5%. The measured enthalpy of solution KCl in water at 298.2 K was 17597±17 J·mol~(-1), enthalpy of reaction of THAM (from NBC-724a in USA) in 0.1000 mol·L~(-1) HCl at 298.2 K was -29779±16J·mol~(-1). The values are in well agreement with the published results. The relability of this calorimeter has been confirmed.
- Themochemistry; Calorimetry; Calorimeter
1. [1]
  Yahui HAN , Jinjin ZHAO , Ning REN , Jianjun ZHANG . Synthesis, crystal structure, thermal decomposition mechanism, and fluorescence properties of benzoic acid and 4-hydroxy-2, 2′: 6′, 2″-terpyridine lanthanide complexes. Chinese Journal of Inorganic Chemistry, 2025, 41(5): 969-982. doi: 10.11862/CJIC.20240395
2. [2]
  Zehua Zhao , Xiaoyan An , Jinrong Xu , Ling Yang , Hao Zhao , Zhongyun Wu . Independent Development and Application of Calorimetric Experiment Data Acquisition and Processing Software. University Chemistry, 2025, 40(11): 402-408. doi: 10.12461/PKU.DXHX202505045
3. [3]
  Yang Lv , Yingping Jia , Yanhua Li , Hexiang Zhong , Xinping Wang . Integrating the Ideological Elements with the “Chemical Reaction Heat” Teaching. University Chemistry, 2024, 39(11): 44-51. doi: 10.12461/PKU.DXHX202402059
4. [4]
  Wenkai Chen , Yunjia Shen , Xiangmeng Kong , Yanli Zeng . Quantum Chemistry Calculation of Key Physical Quantity in Circularly Polarized Luminescence: Introducing an Exploratory Computational Chemistry Experiment. University Chemistry, 2025, 40(3): 83-91. doi: 10.12461/PKU.DXHX202405018
5. [5]
  Jia Zhou . Design and Practice of a Comprehensive Computational Chemistry Experiment Based on High-Throughput Computation and Machine Learning. University Chemistry, 2025, 40(9): 69-75. doi: 10.12461/PKU.DXHX202411067
6. [6]
  Yongqing Xu , Yuyao Yang , Mengna Wu , Xiaoxiao Yang , Xuan Bie , Shiyu Zhang , Qinghai Li , Yanguo Zhang , Chenwei Zhang , Robert E. Przekop , Bogna Sztorch , Dariusz Brzakalski , Hui Zhou . Review on Using Molybdenum Carbides for the Thermal Catalysis of CO₂ Hydrogenation to Produce High-Value-Added Chemicals and Fuels. Acta Physico-Chimica Sinica, 2024, 40(4): 2304003-0. doi: 10.3866/PKU.WHXB202304003
7. [7]
  Tianrong Zhu , Fan Yu , Yuhang Liu , Haiyi Xu , Tingting Ma , Ming Li , Yuhang Xue , Yazhen Wang , Aihua Li , Biao Xiao , Xiaolun Peng . Intelligent Visualization, Precise Iodometry: Color Recognition-based Indirect Iodometric Method for Copper Determination. University Chemistry, 2026, 41(1): 264-275. doi: 10.12461/PKU.DXHX202503096
8. [8]
  Min Hu , Yinghuan Li , Yanhong Bai , Yanping Ren , Juanjuan Song , Yongxian Fan , Dongcheng Liu , Xiuqiong Zeng , Faqiong Zhao , Wenwei Zhang , Mei Shi , Wan Li , Xiuyun Wang , Weihong Li , Xiaohang Qiu , Yong Fan , Jianrong Zhang , Shuyong Zhang . Suggestions on the Method of Hydrothermal-Solventthermal Synthesis and Their Operation Standards. University Chemistry, 2026, 41(3): 208-215. doi: 10.12461/PKU.DXHX202507034
9. [9]
  Lancanghong Chen , Xingtai Yu , Tianlei Zhao , Qizhi Yao . Exploration of Abnormal Phenomena in Iodometric Copper Quantitation Experiment. University Chemistry, 2025, 40(7): 315-320. doi: 10.12461/PKU.DXHX202408089
10. [10]
  Wanzhang Zhang , Yalan Zhong , Chi Huang . Improved Calibration Method for Wet Gas Flowmeters. University Chemistry, 2025, 40(11): 254-262. doi: 10.12461/PKU.DXHX202412121
11. [11]
  Zhuo WANG , Junshan ZHANG , Shaoyan YANG , Lingyan ZHOU , Yedi LI , Yuanpei LAN . Preparation and photocatalytic performance of CeO₂-reduced graphene oxide by thermal decomposition. Chinese Journal of Inorganic Chemistry, 2024, 40(9): 1708-1718. doi: 10.11862/CJIC.20240067
12. [12]
  Yang ZHOU , Lili YAN , Wenjuan ZHANG , Pinhua RAO . Thermal regeneration of biogas residue biochar and the ammonia nitrogen adsorption properties. Chinese Journal of Inorganic Chemistry, 2025, 41(8): 1574-1588. doi: 10.11862/CJIC.20250032
13. [13]
  Jing Kang , Tianyuan Zhao , Qian Zhang , Zhiwen Zhang , Yanyuan Jia , Alideertu Dong . Spotlight on Chlorine: An Innovative Iodometric Method for Visualizing Residual Chlorine. University Chemistry, 2026, 41(3): 343-350. doi: 10.12461/PKU.DXHX202506050
14. [14]
  Limei CHEN , Mengfei ZHAO , Lin CHEN , Ding LI , Wei LI , Weiye HAN , Hongbin WANG . Preparation and performance of paraffin/alkali modified diatomite/expanded graphite composite phase change thermal storage material. Chinese Journal of Inorganic Chemistry, 2024, 40(3): 533-543. doi: 10.11862/CJIC.20230312
15. [15]
  Yuting Bai , Cenqi Yan , Zhen Li , Jiaqiang Qin , Pei Cheng . Preparation of High-Strength Polyimide Porous Films with Thermally Closed Pore Property by In Situ Pore Formation Method. Acta Physico-Chimica Sinica, 2024, 40(9): 2306010-0. doi: 10.3866/PKU.WHXB202306010
16. [16]
  Mengxiu Li , Jiahui Mao , Jiangfeng Ni , Liang Li . Three birds with one stone: modification of Li₅FeO₄ with thermal induction of Lewis acid. Acta Physico-Chimica Sinica, 2026, 42(4): 100189-0. doi: 10.1016/j.actphy.2025.100189
17. [17]
  Zihan Cheng , Kai Jiang , Jun Jiang , Henggang Wang , Hengwei Lin . Achieving thermal-stimulus-responsive dynamic afterglow from carbon dots by singlet-triplet energy gap engineering through covalent fixation. Acta Physico-Chimica Sinica, 2026, 42(2): 100169-0. doi: 10.1016/j.actphy.2025.100169
18. [18]
  Jiaqi Chen , Liang Chen , Xiaocui Wei , Yankai Wang , Yahui Chang , Xinghao Ji , Haoyu Yang , Yue Sun , Yawen Wang , Xiufeng Shi , Xu Wu . Digital Empowerment for Foundational Excellence: A Digitally Enhanced Coordination Titration Experiment of Heating Pack Component Analysis. University Chemistry, 2026, 41(1): 382-393. doi: 10.12461/PKU.DXHX202506008
19. [19]
  Huiying ZHANG , Ping LI , Weixia DONG , Zhiwen HU , Qifu BAO , Qizheng DONG , Mingmin BAI , Wenqi LI . Photocatalytic performance of spheroidal nano Bi₄Ti₃O₁₂ prepared by surfactant-assisted hydrothermal reaction. Chinese Journal of Inorganic Chemistry, 2026, 42(3): 551-561. doi: 10.11862/CJIC.20250269
20. [20]
  Wenwei Zhang , Yiru Wang , Chanzi Ruan , Juanjuan Song , Yongxian Fan , Houjin Li , Dongcheng Liu , Yanping Ren , Xiuqiong Zeng , Faqiong Zhao , Mei Shi , Min Hu , Wan Li , Xiuyun Wang , Weihong Li , Xiaohang Qiu , Yong Fan , Jianrong Zhang , Shuyong Zhang . Suggestions on Heating and Heating Instruments (Part III): Indirect Heating and the Use of Thermal Baths (Water Bath, Oil Bath, Metal Bath and Sand Bath). University Chemistry, 2026, 41(3): 163-171. doi: 10.12461/PKU.DXHX202507039

Get Citation

PDF

XML

Metrics

PDF Downloads(2206)
Abstract views(3256)
HTML views(31)

通讯作者: 陈斌, bchen63@163.com

1.
沈阳化工大学材料科学与工程学院沈阳 110142

Address：Zhongguancun North First Street 2,100190 Beijing, PR China Tel: +86-010-82449177-888

DownLoad: Full-Size Img PowerPoint

Return