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Citation: GUO Xiangyu, ZHAI Junfeng, MA Longhua, WU Qing, BAI Hua, MA Qiang. Rapid on-site screening of five prohibited ingredients in cosmetics using thermal desorption-corona discharge ionization coupled with ion mobility spectrometry[J]. Chinese Journal of Chromatography, ;2019, 37(2): 233-238. doi: 10.3724/SP.J.1123.2018.09005 shu

Rapid on-site screening of five prohibited ingredients in cosmetics using thermal desorption-corona discharge ionization coupled with ion mobility spectrometry

GUO Xiangyu ^1, ,
ZHAI Junfeng ¹ ,
MA Longhua ² ,
WU Qing ² ,
BAI Hua ¹ ,
MA Qiang ¹

1.
Chinese Academy of Inspection and Quarantine, Beijing 100176, China;
2.
Excellims Corporation, Acton, MA 01720, USA

Received Date: 3 September 2018

Fund Project: National Key Research & Development Program of China (No. 2016YFF0203704).

A rapid on-site analytical method is developed for screening lidocaine and four other types of prohibited ingredients in cosmetics using thermal desorption-corona discharge ionization together with ion mobility spectrometry. Performing no pretreatment, we dropped or sprayed cosmetic samples onto a Nomex sampling swab. The sampler was placed into a compartment for thermal desorption and corona discharge ionization; then, ion mobility spectrometry analysis was performed. The limits of detection (LODs) for the five analytes ranged from 10 to 50 ng. The instrumental analysis time for a single run was less than 20 ms, and the total sample analysis period was within 1 min. The proposed method is simple, fast, and has low cost, and could be used as an analytical tool for rapid on-site screening of prohibited ingredients in cosmetics.
- thermal desorption,
- ion mobility spectrometry,
- cosmetics,
- rapid on-site screening
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