Citation: HUANG Li, DAI Yifei, WANG Pingya, ZHOU Yong, ZHAO Qiaoling, JIANG Lingbo, LUO Haijun. Rapid screen of 15 basic artificial dyes in fishery products by ultra performance liquid chromatography coupled with quadrupole-time of flight mass spectrometry[J]. Chinese Journal of Chromatography, ;2015, 33(10): 1097-1103. doi: 10.3724/SP.J.1123.2015.03021 shu

Rapid screen of 15 basic artificial dyes in fishery products by ultra performance liquid chromatography coupled with quadrupole-time of flight mass spectrometry

1.
Zhoushan Institute for Food and Drug Control, Zhoushan Institute of Calibration and Testing for Quality and Technology Supervision, Zhoushan 316021, China

Corresponding author: ZHAO Qiaoling,
Received Date: 17 March 2015

Fund Project: 国家科技部公益专项(201210060) (201210060)舟山市公益类科技项目(2013C31050). (2013C31050)

A new method was established for the simultaneous determination of 15 basic artificial dyes in fishery products by ultra performance liquid chromatography coupled with quadrupole-time of flight mass spectrometry (UPLC-Q-TOF MS). The analytes in fishery products were extracted with acetonitrile containing 10% (v/v) acetic acid, then purified by dispersive solid phase extraction with C₁₈-silicone adsorbent. The compounds were separated by a C₁₈ column with acetonitrile and 0.1% (v/v) formic acid-5 mmol/L ammonium acetate solution as the mobile phases, and measured by UPLC-Q-TOF MS with electrospray ionization in positive mode. As a result, the limits of quantification (LOQs, S/N=10) of the 15 target compounds were 0.1-100 μg/kg in fishery products. The 15 analytes behaved linearly in their respective ranges with the correlation coefficients no less than 0.993. The average recoveries of the 15 analytes spiked at three levels were ranged from 80.60% to 107.37% with the RSDs of 3.33%-6.69% (n=6). This method is suitable for routine qualitative and quantitative analyses of the 15 basic artificial dyes in fishery products due to its fastness, simplicity and relatively high sensitivity.
1. [1]
  [1] Liu S J, Fan M, Jiang N, et al. Chinese Journal of Health Laboratory Technology (刘思洁, 范明, 姜楠, 等. 中国卫生检验杂志), 2013, 23(12): 2593
2. [2]
  [2] Qu Z K, Deng G H, Wang S W, et al. Food Science (屈忠凯, 邓光辉, 王士伟, 等. 食品科学), 2015, 36(4): 217
3. [3]
  [3] Zhang Z L, Mei Y J, Zhang Q M, et al. Chinese Journal of Analysis Laboratory (张贞理, 梅英杰, 张全美, 等. 分析试验室), 2012, 31(4): 15
4. [4]
  [4] Tian X H, Yu Z Q, Chen W, et al. Food Science (田秀慧, 于召强, 陈玮, 等. 食品科学), 2013, 34(12): 171
5. [5]
  [5] Zhu C Y, Wei J, Dong X F, et al. Chinese Journal of Chromatography (朱程云, 魏杰, 董雪芳, 等. 色谱), 2014, 32(4): 419
6. [6]
  [6] Halme K, Lindfors E, Peltonen K. J Chromatogr B, 2007, 845: 74
7. [7]
  [7] Tao Y F, Chen D M, Chao X Q, et al. Food Control, 2011, 22: 1246
8. [8]
  [8] Jing S J, Li J Q. Journal of Shanxi Datong University: Natural Science (景顺杰, 李建晴. 山西大同大学学报: 自然科学版), 2007, 23(3): 22
9. [9]
  [9] Ding C H, Qian L, Ren H H, et al. Food Science (丁长河, 钱林, 任惠华, 等. 食品科学), 2007, 28(2): 244
10. [10]
  [10] Deng G H, Chen S Y, Zhang G H. China Condiment (邓光辉, 陈盛余, 张桂华, 等. 中国调味品), 2011, 36(4): 92
11. [11]
  [11] Song X, Ji S L, Yang L, et al. Chinese Journal of Food Hygiene (宋新, 纪双利, 杨丽, 等. 中国食品卫生杂志), 2009, 21(5): 422
12. [12]
  [12] Xing W W, Wang R M, Wang J Q, et al. Chemical Research and Application (邢玮玮, 王榕妹, 王俊卿, 等. 化学研究与应用), 2010, 22(1): 42
13. [13]
  [13] Zhang H, Chen D Y, Feng J L, et al. Chinese Journal of Health Laboratory Technology (张昊, 陈东洋, 冯家力, 等. 中国卫生检验杂志), 2014, 24(15): 2167
14. [14]
  [14] Yang L, Chen Q J, Ding X R, et al. Science and Technology of Food Industry (杨琳, 陈青俊, 丁献荣, 等. 食品工业科技), 2011, 32(2): 350
15. [15]
  [15] Lin H L, Zhong B P, Hua Y Y. Chinese Journal of Health Laboratory Technology (林宏琳, 钟碧萍, 华永有. 中国卫生检验杂志), 2014, 24(2): 156
16. [16]
  [16] Liu M, Li X L, Bie W, et al. Chinese Journal of Chromatography (刘敏, 李小林, 别玮, 等. 色谱), 2011, 29(2): 162
17. [17]
  [17] Chen Y, Hua J, Pan Y L, et al. China Condiment (陈勇, 花锦, 潘亚利, 等. 中国调味品), 2014, 39(4): 124
18. [18]
  [18] Lin D Q, Wan C B, Qiu P, et al. Journal of Chinese Mass Spectrometry Society (林黛琴, 万承波, 邱萍, 等. 质谱学报), 2013, 34(3): 171
19. [19]
  [19] Zhao Y S, Yang M L, Zhang F, et al. Chinese Journal of Chromatography (赵延胜, 杨敏莉, 张峰, 等. 色谱), 2011, 29(7): 631
20. [20]
  [20] Lü D M, Ding Y L, Zhan S, et al. Modern Instruments & Medical Treatment (吕东明, 丁云连, 詹晟, 等. 现代仪器与医疗), 2013, 19(2): 52
1. [1]
  Zian Lin , Yingxue Jin . Matrix-Assisted Laser Desorption/Ionization Mass Spectrometry (MALDI-MS) for Disease Marker Screening and Identification: A Comprehensive Experiment Teaching Reform in Instrumental Analysis. University Chemistry, 2024, 39(11): 327-334. doi: 10.12461/PKU.DXHX202403066
2. [2]
  Yanhui Zhong , Ran Wang , Zian Lin . Analysis of Halogenated Quinone Compounds in Environmental Water by Dispersive Solid-Phase Extraction with Liquid Chromatography-Triple Quadrupole Mass Spectrometry. University Chemistry, 2024, 39(11): 296-303. doi: 10.12461/PKU.DXHX202402017
3. [3]
  Zhuomin Zhang , Hanbing Huang , Liangqiu Lin , Jingsong Liu , Gongke Li . Course Construction of Instrumental Analysis Experiment: Surface-Enhanced Raman Spectroscopy for Rapid Detection of Edible Pigments. University Chemistry, 2024, 39(2): 133-139. doi: 10.3866/PKU.DXHX202308034
4. [4]
  Jingjie Tang , Luying Xie , Jiayu Liu , Shangyu Shi , Xinyu Sun , Jiayang Lin , Qikun Yang , Chuan'ang Yu , Zecheng Wang , Yingying Wang , Zengyang Xie . Efficient Rapid Synthesis and Antibacterial Activities of Tosylhydrazones: A Recommended Innovative Chemistry Experiment for Undergraduate Medical University. University Chemistry, 2024, 39(3): 316-326. doi: 10.3866/PKU.DXHX202309091
5. [5]
  Ruolin CHENG , Haoran WANG , Jing REN , Yingying MA , Huagen LIANG . Efficient photocatalytic CO₂ cycloaddition over W₁₈O₄₉/NH₂-UiO-66 composite catalyst. Chinese Journal of Inorganic Chemistry, 2024, 40(3): 523-532. doi: 10.11862/CJIC.20230349
6. [6]
  Yuhao SUN , Qingzhe DONG , Lei ZHAO , Xiaodan JIANG , Hailing GUO , Xianglong MENG , Yongmei GUO . Synthesis and antibacterial properties of silver-loaded sod-based zeolite. Chinese Journal of Inorganic Chemistry, 2024, 40(4): 761-770. doi: 10.11862/CJIC.20230169
7. [7]
  Shuang Yang , Qun Wang , Caiqin Miao , Ziqi Geng , Xinran Li , Yang Li , Xiaohong Wu . Ideological and Political Education Design for Research-Oriented Experimental Course of Highly Efficient Hydrogen Production from Water Electrolysis in Aerospace Perspective. University Chemistry, 2024, 39(11): 269-277. doi: 10.12461/PKU.DXHX202403044
8. [8]
  Zhiwen HU , Weixia DONG , Qifu BAO , Ping LI . Low-temperature synthesis of tetragonal BaTiO₃ for piezocatalysis. Chinese Journal of Inorganic Chemistry, 2024, 40(5): 857-866. doi: 10.11862/CJIC.20230462
9. [9]
  Zunxiang Zeng , Yuling Hu , Yufei Hu , Hua Xiao . Analysis of Plant Essential Oils by Supercritical CO₂Extraction with Gas Chromatography-Mass Spectrometry: An Instrumental Analysis Comprehensive Experiment Teaching Reform. University Chemistry, 2024, 39(3): 274-282. doi: 10.3866/PKU.DXHX202309069
10. [10]
  Yufang GAO , Nan HOU , Yaning LIANG , Ning LI , Yanting ZHANG , Zelong LI , Xiaofeng LI . Nano-thin layer MCM-22 zeolite: Synthesis and catalytic properties of trimethylbenzene isomerization reaction. Chinese Journal of Inorganic Chemistry, 2024, 40(6): 1079-1087. doi: 10.11862/CJIC.20240036
11. [11]
  Tianlong Zhang , Xinyuan Zhang , Xing Zhao , Hongsheng Tang , Yan Li , Hua Li . Colors of Dotted Stone: The Colorful World of Dunhuang Murals. University Chemistry, 2024, 39(6): 238-245. doi: 10.3866/PKU.DXHX202401047
12. [12]
  Di Yang , Jiayi Wei , Hong Zhai , Xin Wang , Taiming Sun , Haole Song , Haiyan Wang . Rapid Detection of SARS-CoV-2 Using an Innovative “Magic Strip”. University Chemistry, 2024, 39(4): 373-381. doi: 10.3866/PKU.DXHX202312023
13. [13]
  Chunyang Zheng , Shiyu Liu , Nuo Yi , Hong Shang . The Adventures in the Kingdom of Plant Pigments. University Chemistry, 2024, 39(9): 170-176. doi: 10.3866/PKU.DXHX202308085
14. [14]
  Wei Zhong , Dan Zheng , Yuanxin Ou , Aiyun Meng , Yaorong Su . K原子掺杂高度面间结晶的g-C₃N₄光催化剂及其高效H₂O₂光合成. Acta Physico-Chimica Sinica, 2024, 40(11): 2406005-. doi: 10.3866/PKU.WHXB202406005
15. [15]
  Guoqiang Chen , Zixuan Zheng , Wei Zhong , Guohong Wang , Xinhe Wu . 熔融中间体运输导向合成富氨基g-C₃N₄纳米片用于高效光催化产H₂O₂. Acta Physico-Chimica Sinica, 2024, 40(11): 2406021-. doi: 10.3866/PKU.WHXB202406021
16. [16]
  Ziliang KANG , Jiamin ZHANG , Hong AN , Xiaohua LIU , Yang CHEN , Jinping LI , Libo LI . Preparation and water adsorption properties of CaCl₂@MOF-808 in-situ composite moulded particles. Chinese Journal of Inorganic Chemistry, 2024, 40(11): 2133-2140. doi: 10.11862/CJIC.20240282
17. [17]
  Min Gu , Huiwen Xiong , Liling Liu , Jilie Kong , Xueen Fang . Rapid Quantitative Detection of Procalcitonin by Microfluidics: An Instrumental Analytical Chemistry Experiment. University Chemistry, 2024, 39(4): 87-93. doi: 10.3866/PKU.DXHX202310120
18. [18]
  Shitao Fu , Jianming Zhang , Cancan Cao , Zhihui Wang , Chaoran Qin , Jian Zhang , Hui Xiong . Study on the Stability of Purple Cabbage Pigment. University Chemistry, 2024, 39(4): 367-372. doi: 10.3866/PKU.DXHX202401059
19. [19]
  Feiya Cao , Qixin Wang , Pu Li , Zhirong Xing , Ziyu Song , Heng Zhang , Zhibin Zhou , Wenfang Feng . Magnesium-Ion Conducting Electrolyte Based on Grignard Reaction: Synthesis and Properties. University Chemistry, 2024, 39(3): 359-368. doi: 10.3866/PKU.DXHX202308094
20. [20]
  Pei Li , Yuenan Zheng , Zhankai Liu , An-Hui Lu . Boron-Containing MFI Zeolite: Microstructure Control and Its Performance of Propane Oxidative Dehydrogenation. Acta Physico-Chimica Sinica, 2025, 41(4): 100034-. doi: 10.3866/PKU.WHXB202406012

Get Citation

PDF

XML

Metrics

PDF Downloads(0)
Abstract views(274)
HTML views(8)

通讯作者: 陈斌, bchen63@163.com

1.
沈阳化工大学材料科学与工程学院沈阳 110142