Citation: Mohammad ASADI, Ali Mohammad HAJI SHABANI, Shayessteh DADFARNIA, Bijan ABBASI. Solidified floating organic drop microextraction combined with high performance liquid chromatography for the determination of carbamazepine in human plasma and urine samples[J]. Chinese Journal of Chromatography, ;2015, 33(6): 634-641. doi: 10.3724/SP.J.1123.2015.02072 shu

Solidified floating organic drop microextraction combined with high performance liquid chromatography for the determination of carbamazepine in human plasma and urine samples

1.
1. Department of Chemistry, Faculty of Science, Yazd University, Yazd 89195-741, Iran;

Corresponding author: Shayessteh DADFARNIA,
Received Date: 11 February 2015

Solidified floating organic drop microextraction (SFODME) in combination with high performance liquid chromatography was used for separation/preconcentration and determination of carbamazepine (CBZ) in human plasma and urine samples. Parameters that affect the extraction efficiency such as the type and volume of extraction solvent, ionic strength, sodium hydroxide concentration, stirring rate, sample volume and extraction time, were investigated and optimized. Under the optimum conditions (extraction solvent, 40 μL of 1-undecanol; sodium hydroxide concentration, 1 mol/L; temperature, 50 ℃; stirring speed, 400 r/min; sample volume, 8 mL; sodium chloride concentration, 3% (w/v) and extraction time, 60 min) the calibration curve was found to be linear in the mass concentration range of 0.4-700.0 μg/L. The limit of detection (LOD) was 0.1 μg/L and the relative standard deviation (RSD) for six replicate extraction and determination of carbamazepine at 100 μg/L level was found to be 4.1%. The method was successfully applied to the determination of CBZ in human plasma and urine samples.
- solidified floating organic drop microextraction (SFODME),
- high performance liquid chromatography (HPLC),
- carbamazepine (CBZ),
- plasma,
- urine,
- preconcentration
1. [1]
  [1] Bernus I, Dickinson R G, Hooper W D, et al. Epilepsy Res, 1996, 24: 163
2. [2]
  [2] Deleu D, Aarons L, Ahmed I A. Eur J Clin Pharmacol, 2001, 57(3): 243
3. [3]
  [3] Albani F, Riva R, Baruzzi A. Pharmacopsychiatry, 1995, 28: 235
4. [4]
  [4] Yoshida T, Imai K, Motohashi S, et al. J Pharm Biomed Anal, 2006, 41(4): 1386
5. [5]
  [5] Duzova A, Baskin E, Usta Y, et al. Hum Exp Toxicol, 2001, 20(4): 175
6. [6]
  [6] Alexishvili M M, Rukhadze M D, Okujava V M. Biomed Chromatogr, 1997, 11(1): 36
7. [7]
  [7] Fortuna A, Bicker J, Alves G, et al. J Sep Sci, 2011, 34(12): 1391
8. [8]
  [8] Messiha F S. Alcohol, 1986, 3(2): 135
9. [9]
  [9] Miao X S, Metcalfe C D. Anal Chem, 2003, 75(15): 3731
10. [10]
  [10] Kim K B, Seo K A, Kim S E, et al. J Pharm Biomed Anal, 2011, 56(4): 771
11. [11]
  [11] Zhu Y X, Chiang H, Wulster-Radcliffe M, et al. J Pharm Biomed Anal, 2005, 38(1): 119
12. [12]
  [12] Wu J, Xiang B, Xia J. Microchim Acta, 2009, 166(1/2): 157
13. [13]
  [13] Junk G A, Richard J. Anal Chem, 1988, 60(5): 451
14. [14]
  [14] Liu S, Dasgupta P K. Anal Chem, 1995, 67(13): 2042
15. [15]
  [15] Liu S, Dasgupta P K. Anal Chem, 1996, 68(11): 1817
16. [16]
  [16] Jeannot M A, Cantwell F F. Anal Chem, 1996, 68(13): 2236
17. [17]
  [17] He Y, Lee H K. Anal Chem, 1997, 69(22): 4634
18. [18]
  [18] Piroozi F, Ghasemi E, Qomi M, et al. J Liq Chromatogr Relat Technol, 2014, 37(5): 760
19. [19]
  [19] Tian J, Chen X, Bai X H. Chinese Journal of Chromatography, 2012, 30(5): 507
20. [20]
  [20] Farajzadeh M A, Bahram M, Zorita S, et al. J Hazard Mater, 2009, 161(2/3): 1535
21. [21]
  [21] Rezaee M, Mashayekhi H A, Mohammad Hosseini M, et al. J Liq Chromatogr Relat Technol, 2014, 37(18): 2559
22. [22]
  [22] Xiaohuan Z, Guijiang Z, Chun W, et al. Chinese Journal of Chromatography, 2015, 33(2): 103
23. [23]
  [23] Wang P, Qiu X, Yang Y. J Liq Chromatogr Relat Technol, 2015, 38(5): 640
24. [24]
  [24] Farajzadeh M A, Djozan D J, Bakhtiyari R F. Talanta, 2010, 81(4/5): 1360
25. [25]
  [25] Farajzadeh M R, Seyedi S E, Safi Shalamzari M, et al. J Sep Sci, 2009, 32(18): 3191
26. [26]
  [26] Leong M I, Huang S D. J Chromatogr A, 2008, 1211(1/2): 8
27. [27]
  [27] Dadfarnia S, HajiShabani A M. Anal Chim Acta, 2010, 658: 107
28. [28]
  [28] Rohani Moghadam M, Dadfarnia S, Haji Shabani A M. J Hazard Mater, 2011, 186(1): 169
29. [29]
  [29] Dadfarnia S, Haji Shabani A M, Kamranzadeh E. Talanta, 2009, 79(4): 1061
30. [30]
  [30] Suh J H, Lee Y Y, Lee H J, et al. J Pharm Biomed Anal, 2013, 75: 214
31. [31]
  [31] Adlnasab L, Ebrahimzadeh H, Yamini Y, et al. Talanta, 2010, 83: 370
32. [32]
  [32] Bagheri H, Saber A, Mousavi S R. J Chromatogr A, 2004, 1046(1/2): 27
33. [33]
  [33] Besharati-Seidani A, Jabbari A, Yamini Y. Anal Chim Acta, 2005, 530(1): 155
34. [34]
  [34] Al-Hadithi N, Saad B, Grote M. Microchim Acta, 2011, 172: 31
35. [35]
  [35] Ferreira A, Rodrigues M, Oliveira P, et al. J Chromatogr B, 2014, 971: 20
36. [36]
  [36] Cantú M D, Toso D R, Lacerda C A, et al. Bioanal Chem, 2006, 386: 256
37. [37]
  [37] Rezaee M, Mashayekhi H A. Anal Methods, 2012, 4: 2887
38. [38]
  [38] Mashayekhi H A, Abroomand-Azar P, Saber-Tehrani M, et al. Chromatographia, 2010, 71: 517
39. [39]
  [39] Behbahani M, Najafi F, Bagheri S, et al. J Chromatogr A, 2013, 1308: 25
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