Citation: YAN Kuanglin, LIN Liqiong, ZHENG Xiaxi, XIAO Xiaohua, CAO Yujuan. Progress of sample preparation techniques in gas chromatographic analysis[J]. Chinese Journal of Chromatography, ;2013, 31(7): 634-639. doi: 10.3724/SP.J.1123.2013.05035 shu

Progress of sample preparation techniques in gas chromatographic analysis

1.
1. School of Chemistry and Chemical Engineering, Sun Yan-sen University, Guangzhou 510275, China;

Corresponding author: XIAO Xiaohua, CAO Yujuan,
Received Date: 22 May 2013

Fund Project: 广东省自然科学基金项目(S2012010010787). (S2012010010787)

Gas chromatography (GC) is a widely used analytical technique in many fields. Sample preparation is very important in GC analysis due to its time consumed and deviations produced. In the present paper, the progress of some typical sample preparation techniques in gas chromatography, including purge and trap, solid phase extraction, solid phase microextraction, liquid phase microextraction, microwave assisted extraction, ultrasonic-assisted extraction, etc., are reviewed.
- sample preparation,
- gas chromatography (GC),
- review
1. [1]
  [1] Ruiz-Bevia F, Fernandez-Torres M J, Blasco-Alemany M P. Anal Chim Acta, 2009, 632: 304
2. [2]
  [2] Soria A C, Martinez-Castro I, Sanz J. J Chromatogr A, 2009, 1216: 3300
3. [3]
  [3] Barco-Bonilla N, Plaza-Bolanos P, Fernandez-Moreno J L, et al. Anal Bioanal Chem, 2011, 400: 3537
4. [4]
  [4] Deng X, Liang G, Chen J, et al. J Chromatogr A, 2011, 1218: 3791
5. [5]
  [5] Jimenez J J. Anal Chim Acta, 2013, 770: 94
6. [6]
  [6] Muller K, Seubert A. J Chromatogr A, 2012, 1260: 9
7. [7]
  [7] Ma J, Xiao R, Li J, et al. J Chromatogr A, 2010, 1217: 5462
8. [8]
  [8] Zhang H, Low W P, Lee H K. J Chromatogr A, 2012, 1233: 16
9. [9]
  [9] Peng X T, Zhao X, Feng Y Q. J Chromatogr A, 2011, 1218: 9314
10. [10]
  [10] Santos M G, Vitor R V, Andrade F L, et al. J Chromatogr B, 2012, 909: 70
11. [11]
  [11] Song X L, Li J H, Xu S F, et al. Talanta, 2012, 99: 75
12. [12]
  [12] Labadie P, Alliot F, Boourges C, et al. Anal Chim Acta, 2010, 675: 97
13. [13]
  [13] Garcia-Fodriguez D, Cela-Torrijos R, Lorenzo-Ferreira R A, et al. Food Chem, 2012, 135: 259
14. [14]
  [14] Su R, Wang X H, Xu X, et al. J Chromatogr A, 2011, 1218: 5047
15. [15]
  [15] Aquino A, Ferreira J A, Navickiene S, et al. J AOAC Int, 2012, 95: 1338
16. [16]
  [16] Moliner-Martinez Y, Campins-Falco P, Molins-Legua C, et al. J Chromatogr A, 2009, 1216: 6741
17. [17]
  [17] Kenessov B N, Koziel J A, Grotenhuis T, et al. Anal Chim Acta, 2010, 674: 32
18. [18]
  [18] de Morais P, Stoichev T, Basto M C P, et al. Anal Bioanal Chem, 2011, 399: 2531
19. [19]
  [19] Riu-Aumatell M, Vargas L, Vichi S, et al. Food Chem, 2011, 129: 557
20. [20]
  [20] Ho T T, Chen C Y, Li Z G, et al. Anal Chim Acta, 2012, 712: 72
21. [21]
  [21] Amini R, Rouhollahi A, Adibi M, et al. J Chromatogr A, 2011, 1218: 130
22. [22]
  [22] Sarafraz-Yazdi A, Abbasian M, Amiri A. Food Chem, 2012, 131: 698
23. [23]
  [23] Chen X F, Zang H, Wang X, et al. Analyst, 2012, 137: 5411
24. [24]
  [24] Liu W, Zhang L, Fan L B, et al. J Chromatogr A, 2012, 1233: 1
25. [25]
  [25] Jeannot M A, Cantwell F F. Anal Chem, 1996, 68(13): 2236
26. [26]
  [26] Cortada C, Vidal L, Tejada S, et al. Anal Chim Acta, 2009, 638: 29
27. [27]
  [27] Li Y, Xiong Y Q, Liang Q Y, et al. J Chromatogr A, 2010, 1217: 3561
28. [28]
  [28] Yu Y J, Chen B, Shen C, et al. J Chromatogr A, 2010, 1217: 5158
29. [29]
  [29] Almeida C, Femandes J O, Cunha S C. Food Control, 2012, 25: 380
30. [30]
  [30] Pusvaskiene E, Januskevic B, Prichodko A, et al. Chromatographia, 2009, 69: 271
31. [31]
  [31] Zhao R S, Diao C P, Chen Q F, et al. J Sep Sci, 2009, 32: 1069
32. [32]
  [32] Aguilera-Herrador E, Lucena R, Cardenas S, et al. J Chromatogr A, 2009, 1216: 5580
33. [33]
  [33] Chisvert A, Roman I P, Vidal L, et al. J Chromatogr A, 2009, 1216: 1290
34. [34]
  [34] Sanchez-Brunete C, Miguel E, Albero B, et al. J Chromatogr A, 2010, 1217: 7024
35. [35]
  [35] Salemi A, Rasoolzadeh R, Nejad M M, et al. Anal Chim Acta, 2013, 769: 121
36. [36]
  [36] Yan H Y, Liu B M, Du J J, et al. Analyst, 2010, 135: 2585
37. [37]
  [37] Wang L, Wang L L, Chen J, et al. J Chromatogr A, 2012, 1256: 9
38. [38]
  [38] Wang L, Wang Z M, Zhang H H, et al. Anal Chim Acta, 2009, 647: 72
39. [39]
  [39] Bowden J A, Colosi D M, Stutts W L, et al. Anal Chem, 2009, 81: 6725
40. [40]
  [40] Coscolla C, Castillo M, Pastor A, et al. Anal Chim Acta, 2011, 693: 72
41. [41]
  [41] Liu R L, Zhang J, Mou Z L, et al. Analyst, 2012, 137: 5135
42. [42]
  [42] Azzouz A, Ballesteros E. J Chromatogr B, 2012, 891/892: 12
43. [43]
  [43] Ponnusamy V K, Jen J F. J Chromatogr A, 2011, 1218: 6861
44. [44]
  [44] Huang M C, Chen H C, Fu S C, et al. Food Chem, 2013, 138: 227
45. [45]
  [45] Gholivand M B, Abolghasemi M M, Piryaei M, et al. Food Chem, 2013, 138: 251
46. [46]
  [46] Deng X W, Xie P, Qi M, et al. J Chromatogr A, 2012, 1219: 75
47. [47]
  [47] Zhou T, Xiao X H, Li G K. Anal Chem, 2012, 84: 5816
48. [48]
  [48] Zhou T, Xiao X H, Li G K. Anal Chem, 2012, 84: 420
49. [49]
  [49] Chikushi H, Fujii Y, Toda K. J Chromatogr A, 2012, 1256: 267
50. [50]
  [50] Yang T J, Tsai F J, Chen C Y, et al. Anal Chim Acta, 2010, 668: 188
51. [51]
  [51] Liu W L, Hwang B H, Li Z G, et al. J Chromatogr A, 2011, 1218: 7857
52. [52]
  [52] Aragon M, Marce R M, Borrull F. Talanta, 2012, 101: 473
53. [53]
  [53] Ramirez N, Marce R M, Borrull F. J Chromatogr A, 2011, 1218: 6226
54. [54]
  [54] Llpo A, Borrull F, Pocurull E. Talanta, 2012, 88: 284
55. [55]
  [55] Shi X Z, Song S Q, Sun A L, et al. Analyst, 2012, 137: 437
56. [56]
  [56] Posada-Ureta O, Olivares M, Navarro P, et al. J Chromatogr A, 2012, 1227: 38
57. [57]
  [57] Cacho J I, Campillo N, Vinas P, et al. J Chromatogr A, 2013, 1279: 1
58. [58]
  [58] Stadler S, Stefanuto P H, Brokl M, et al. Anal Chem, 2013, 85(S1): 998
59. [59]
  [59] Xu X M, Yu S, Li R, et al. Food Chem, 2012, 135: 161
60. [60]
  [60] Hou X, Han M, Dai X H, et al. Food Chem, 2013, 138: 1198
1. [1]
  Ying Chen , Ronghua Yan , Weiyan Yin . Research Progress on the Synthesis of Metal Single-Atom Catalysts and Their Applications in Electrocatalytic Hydrogen Evolution Reactions. University Chemistry, 2025, 40(9): 344-353. doi: 10.12461/PKU.DXHX202503066
2. [2]
  .
  CCS Chemistry 综述推荐│绿色氧化新思路：光/电催化助力有机物高效升级
  . CCS Chemistry, 2025, 7(10.31635/ccschem.024.202405369): -.
3. [3]
  Yifan Liu , Haonan Peng . AI-Assisted New Era in Chemistry: A Review of the Application and Development of Artificial Intelligence in Chemistry. University Chemistry, 2025, 40(7): 189-199. doi: 10.12461/PKU.DXHX202405182
4. [4]
  Zunxiang Zeng , Yuling Hu , Yufei Hu , Hua Xiao . Analysis of Plant Essential Oils by Supercritical CO₂Extraction with Gas Chromatography-Mass Spectrometry: An Instrumental Analysis Comprehensive Experiment Teaching Reform. University Chemistry, 2024, 39(3): 274-282. doi: 10.3866/PKU.DXHX202309069
5. [5]
  Shunü Peng , Huamin Li , Zhaobin Chen , Yiru Wang . Simultaneous Application of Multiple Quantitative Analysis Methods in Gas Chromatography for the Determination of Active Ingredients in Traditional Chinese Medicine Preparations. University Chemistry, 2025, 40(10): 243-249. doi: 10.12461/PKU.DXHX202412043
6. [6]
  Xiaowu Zhang , Pai Liu , Qishen Huang , Shufeng Pang , Zhiming Gao , Yunhong Zhang . Acid-Base Dissociation Equilibrium in Multiphase System: Effect of Gas. University Chemistry, 2024, 39(4): 387-394. doi: 10.3866/PKU.DXHX202310021
7. [7]
  Runjie Li , Hang Liu , Xisheng Wang , Wanqun Zhang , Wanqun Hu , Kaiping Yang , Qiang Zhou , Si Liu , Pingping Zhu , Wei Shao . 氨基酸的衍生及手性气相色谱分离创新实验. University Chemistry, 2025, 40(6): 286-295. doi: 10.12461/PKU.DXHX202407059
8. [8]
  Jiao CHEN , Yi LI , Yi XIE , Dandan DIAO , Qiang XIAO . Vapor-phase transport of MFI nanosheets for the fabrication of ultrathin b-axis oriented zeolite membranes. Chinese Journal of Inorganic Chemistry, 2024, 40(3): 507-514. doi: 10.11862/CJIC.20230403
9. [9]
  Yanhui Zhong , Ran Wang , Zian Lin . Analysis of Halogenated Quinone Compounds in Environmental Water by Dispersive Solid-Phase Extraction with Liquid Chromatography-Triple Quadrupole Mass Spectrometry. University Chemistry, 2024, 39(11): 296-303. doi: 10.12461/PKU.DXHX202402017
10. [10]
  Ke Qiu , Fengmei Wang , Mochou Liao , Kerun Zhu , Jiawei Chen , Wei Zhang , Yongyao Xia , Xiaoli Dong , Fei Wang . A Fumed SiO₂-based Composite Hydrogel Polymer Electrolyte for Near-Neutral Zinc-Air Batteries. Acta Physico-Chimica Sinica, 2024, 40(3): 2304036-0. doi: 10.3866/PKU.WHXB202304036
11. [11]
  Yuanchun Pan , Xinyun Lin , Leyi Yang , Wenya Hu , Dekui Song , Nan Liu . Artificial Intelligence Science Practice: Preparation of Electronic Skin by Chemical Vapor Deposition of Graphene. University Chemistry, 2025, 40(11): 272-280. doi: 10.12461/PKU.DXHX202412052
12. [12]
  Yifan Xie , Liyun Yao , Ruolin Yang , Yuxing Cai , Yujie Jin , Ning Li . Exploration and Practice of Online and Offline Hybrid Teaching Mode in High-Performance Liquid Chromatography Experiment. University Chemistry, 2025, 40(11): 100-107. doi: 10.12461/PKU.DXHX202412133
13. [13]
  Zufeng Qiu , Jie Ouyang , Yiru Wang , Hengting Yang , Xin Liao , Chi Zhang , Xuanyao Jiang , Shunliu Deng , Zhiwei Lin . 综合运用分析仪器解析“盲盒”样品——未知物的剖析. University Chemistry, 2025, 40(6): 296-302. doi: 10.12461/PKU.DXHX202405167
14. [14]
  Fa Wang , Yu Chen , Hui Chao . Ruthenium(II) Complexes as Photoactivated Chemo-Prodrugs for Hypoxic Tumor Therapy. University Chemistry, 2025, 40(7): 200-212. doi: 10.12461/PKU.DXHX202410024
15. [15]
  Jing Wang , Pingping Li , Yuehui Wang , Yifan Xiu , Bingqian Zhang , Shuwen Wang , Hongtao Gao . Treatment and Discharge Evaluation of Phosphorus-Containing Wastewater. University Chemistry, 2024, 39(5): 52-62. doi: 10.3866/PKU.DXHX202309097
16. [16]
  Zhongyan Cao , Shengnan Jin , Yuxia Wang , Yiyi Chen , Xianqiang Kong , Yuanqing Xu . Advances in Highly Selective Reactions Involving Phenol Derivatives as Aryl Radical Precursors. University Chemistry, 2025, 40(4): 245-252. doi: 10.12461/PKU.DXHX202405186
17. [17]
  Zhaohu Li , Weidong Wang , Yuhao Liu , Mingzhe Han , Lingling Wei , Huan Jiao . Research on the Safety Management and Disposal of Chemical Laboratory Waste. University Chemistry, 2024, 39(10): 128-136. doi: 10.3866/PKU.DXHX202312090
18. [18]
  Zehua Zhao , Xiaoyan An , Jinrong Xu , Ling Yang , Hao Zhao , Zhongyun Wu . Independent Development and Application of Calorimetric Experiment Data Acquisition and Processing Software. University Chemistry, 2025, 40(11): 402-408. doi: 10.12461/PKU.DXHX202505045
19. [19]
  Lisen Sun , Yongmei Hao , Zhen Huang , Yongmei Liu . Experimental Teaching Design for Viscosity Measurement Serves the Optimization of Operating Conditions for Kitchen Waste Treatment Equipment. University Chemistry, 2024, 39(2): 52-56. doi: 10.3866/PKU.DXHX202307063
20. [20]
  Kun Xu , Xinxin Song , Zhilei Yin , Jian Yang , Qisheng Song . Comprehensive Experimental Design of Preferential Orientation of Zinc Metal by Heat Treatment for Enhanced Electrochemical Performance. University Chemistry, 2024, 39(4): 192-197. doi: 10.3866/PKU.DXHX202309050

Get Citation

PDF

XML

Metrics

PDF Downloads(0)
Abstract views(559)
HTML views(65)

通讯作者: 陈斌, bchen63@163.com

1.
沈阳化工大学材料科学与工程学院沈阳 110142