Citation: MA Zhen-Zhen, WANG Li-Qin, ZHANG Ya-Xu, YOU Rui, GUO Zhi-Tong, YANG Lu. Morphological and Structural Study of Several Polychromy Artworks Proteinaceous Binders after Soil Aging[J]. Chinese Journal of Analytical Chemistry, ;2020, 48(7): 896-902. doi: 10.19756/j.issn.0253-3820.191620 shu

Morphological and Structural Study of Several Polychromy Artworks Proteinaceous Binders after Soil Aging

MA Zhen-Zhen ^1,2, ,
WANG Li-Qin ^1,3 ,
ZHANG Ya-Xu ^1,2 ,
YOU Rui ¹ ,
GUO Zhi-Tong ¹ ,
YANG Lu ^1,3

1.
School of Cultural Heritage, Northwest University, Xi'an 710069, China;
2.
Shaanxi Academy of Archaeology, Xi'an 710054, China;
3.
Key Laboratory of Cultural Heritage Research and Conservation, Ministry of Education, Northwest University, Xi'an 710069, China

Received Date: 21 October 2019
Revised Date: 27 April 2020

Fund Project: This work was supported by the National Key R&D Program of China (No. 2019YFC1520100), the Key Industry Innovation Chain (Group) Project of Shaanxi Province (No. 2019ZDLSF07-05), the Key Scientific and Technological Team from Innovation Shaanxi Province (No. 2015KCT-12) and the Cultural Relics Protection Project of Shaanxi Provincial Cultural Heritage Administration (No. 2019-012).

For overall study of the soil aging influence on the common polychromy artworks proteinaceous binders, scanning electron microcopy, X-ray diffraction and infrared spectroscopy were applied to characterize the morphology, crystallinity, and proteins secondary structure contents of the common-used five binders (pig glue, whole egg, egg white, egg yolk and milk) in ancient China before and after soil aging. The results illustrated that the regular structures had deteriorated to the loosing states. The crystallinity all decreased, with milk declining the most. The binders still possessed the stair-stepped amide I, Ⅱ, Ⅲ FTIR absorbance while the helical structures had dissociated. Moreover, the content of α-helix declined while those at of β-sheet and random coils climbed, suggesting binders' structures had transformed to unordered states.
- Morphology,
- Structure,
- Soil aging,
- Proteinaceous binder,
- Polychromy artwork
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