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Citation: Sheng-Jun Xu, Ya-Nan Zhou, Guo-Ping Shen, Bin Dong. Ni(OH)2 Derived from NiS2 Induced by Reflux Playing Three Roles for Hydrogen/Oxygen Evolution Reaction[J]. Chinese Journal of Structural Chemistry, ;2022, 41(8): 220805. doi: 10.14102/j.cnki.0254-5861.2022-0143 shu

Ni(OH)2 Derived from NiS2 Induced by Reflux Playing Three Roles for Hydrogen/Oxygen Evolution Reaction

  • 1.

    Dongying Haike Ruilin Chemical Co., LTD., Dongying 257000, China

  • 2.

    State Key Laboratory of Heavy Oil Processing, College of Chemistry and Chemical Engineering, China University of Petroleum (East China), Qingdao 266580, China

Figures(6)

  • Developing efficient and promising non-noble catalysts for oxygen evolution reaction (OER) and hydrogen evolution reaction (HER) is vital but still a huge challenge for the clean energy system. Herein, we have integrated the active components for OER (Ni(OH)2) and HER (NiS2 and Ni(OH)2) into Ni(OH)2@NiS2 heterostructures by a facile reflux method. The in-situ formed Ni(OH)2 thin layer is coated on the surface of hollow NiS2 nanosphere. The uniform Ni(OH)2@NiS2 hollow sphere processes enlarge the electrochemically active specific surface area and enhance the intrinsic activity compared to NiS2 precursor, which affords a current density of 10 mA cm-2 at the overpotential of 309 mV and 100 mA cm-2 at 359 mV for OER. Meanwhile, Ni(OH)2@NiS2 can reach 10 mA cm-2 at 233 mV for HER, superior to pure NiS2. The enhanced performance can be attributed to the synergy between Ni(OH)2 and NiS2. Specifically, Ni(OH)2 has three functions for water splitting: providing active sites for hydrogen adsorption and hydroxyl group desorption and working as real OER active sites. Moreover, Ni(OH)2@NiS2 displays great stability for OER (50 h) and HER (30 h).
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