Citation: HU Biao, YU Di, HUANG Kai, YU Shu-Juan. Metal-ion Interactions with Sugars: Crystal Structure of Bis(4-dehydro-L-arabinose) Calcium Methanol Bishydrate[J]. Chinese Journal of Structural Chemistry, ;2015, 34(5): 764-770. doi: 10.14102/j.cnki.0254-5861.2011-0517
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The crystal structure of the metal-organic frame Ca(C5H9O5)2·CH3OH·2H2O (1) has been synthesized and characterized. Complex 1 belongs to a tetragonal P43212 space group. In complex 1, the sugar moiety shows a beta-L configuration of pyranose form. The calcium(II) is eight-coordinated, binding to four such sugar moieties, via O(1), O(2) of two molecules and O(3), O(4) of the other two, with the 4-hydroxy group being deprotonated. The water and methanol molecules are not coordinated to the calcium ion.
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