Citation: ZHAO Peng, LIU Yun, HONG Huan-Huan, WEN Lu-Hong, SHI Zhen-Zhi, ZHANG Xin-Rong, ZHANG Si-Chun, LI Xue-Jun. Fast Analysis of Veterinary Drugs in Feed Using Gold Nanoparticles-assisted Dielectric Barrier Discharge Ion Source-Mass Spectrometry[J]. Chinese Journal of Analytical Chemistry, ;2018, 46(7): 1089-1094. doi: 10.11895/j.issn.0253-3820.181099 shu

Fast Analysis of Veterinary Drugs in Feed Using Gold Nanoparticles-assisted Dielectric Barrier Discharge Ion Source-Mass Spectrometry

1.
The Research Institute of Advanced Technologies, Ningbo University, Ningbo 315211, China;
2.
Department of Chemistry, Tsinghua University, Beijing 100084, China;
3.
Yingkou Entry-Exit Inspection and Quarantine Bureau, Yingkou 115004, China

Received Date: 5 February 2018
Revised Date: 16 May 2018

Fund Project: This work was supported by the National Key Scientific Instrument and Equipment Development Project (No. 2016YFF0100300), the National Natural Science Foundation of China (No.51605231), the Ningbo Municipal Natural Science Foundation (No. 2016A610055), the Ningbo Municipal Natural Science Foundation (No. 2017A610164) and the K.C. Wong Magna Fund in Ningbo University, China.

Dielectric barrier discharge ion source-mass spectrometry (DBDI-MS) can achieve in-situ and efficient detection of samples without tedious pretreatment, and has become a popular analytical method. To improve the detection sensitivity, a novel mass spectrometric method based on gold nanoparticles (AuNPs)-assisted paper-based injection mode and DBDI-MS technology was developed for the fast determination of four veterinary drugs. The detection signal strength was improved by 8-31 times compared to the veterinary drugs which were tested without AuNPs-assisted paper based injection. Under the optimal conditions, the experimental data of four veterinary drugs showed a good linear relationship between the signal and the concentration in the respective range, with correlation coefficient (r) of 0.951-0.996. Moreover, the recoveries were between 79.4% and 96.5% at three spiked levels. This method has many distinct advantages, such as low detected limitation, low cost and high efficiency, and is also very suitable for fast on-site detecting, showing great potential in feed quality control.
- Dielectric barrier discharge ion source-mass spectrometry,
- Paper-based injection,
- Gold nanoparticles,
- Veterinary drug
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