Citation: JIANG Bin, HE Xiao-Min, YANG Yun-Huang, ZHANG Xu, ZHOU Xin, LI Cong-Gang, YANG Dai-Wen, LIU Mai-li. Suppress Sampling Truncation Artifacts in Constant-time Type Nuclear Magnetic Resonance Experiments Using Iterative Soft Thresholding Method[J]. Chinese Journal of Analytical Chemistry, ;2017, 45(12): 1888-1894. doi: 10.11895/j.issn.0253-3820.171218 shu

Suppress Sampling Truncation Artifacts in Constant-time Type Nuclear Magnetic Resonance Experiments Using Iterative Soft Thresholding Method

JIANG Bin ¹ ,
HE Xiao-Min ² ,
YANG Yun-Huang ¹ ,
ZHANG Xu ¹ ,
ZHOU Xin ¹ ,
LI Cong-Gang ¹ ,
YANG Dai-Wen ^3,, ,
LIU Mai-li ^1,,

1.
State Key Laboratory of Magnetic Resonance and Atomic and Molecular Physics, Wuhan Institute of Physics and Mathematics, the Chinese Academy of Sciences, Wuhan 430071, China
2.
College of Chemistry, Central China Normal University, Wuhan 430079, China
3.
Department of Biological Sciences, National University of Singapore, Singapore, 117543

Corresponding author: YANG Dai-Wen, dbsydw@nus.edu.sg LIU Mai-li, ml.liu@wipm.ac.cn
Received Date: 1 September 2017
Accepted Date: 2 November 2017

Fund Project: This work was supported by the National Key R & D Program of China (Nos. 2017YFA0505400, 2016YFA051201), the National Natural Science Foundation of China (Nos. 21735007, 21475146, 81227902, 21675170)the National Key R & D Program of China 2017YFA0505400the National Natural Science Foundation of China 21675170the National Natural Science Foundation of China 81227902the National Natural Science Foundation of China 21735007the National Key R & D Program of China 2016YFA051201the National Natural Science Foundation of China 21475146

Figures(5)

Sampling truncation, i.e. sampling ends before signal decays to zero, introduces wiggle-like artifacts that impair the quality of nuclear magnetic resonance (NMR) spectra. In multidimensional (mD) NMR experiments, the first few hundred or less data points are commonly sampled in the indirect dimension, and the truncation is unavoidable. Apodization can suppress truncation artifacts with cost of line-broadening. Linear prediction is also beneficial to the reduction of truncation artifacts. The worst situation is in the constant time (CT) type experiments, where the signal doesn't decay at all in the CT evolution dimension. In this contribution we proposed that, although iterative soft thresholding (IST) was rarely used due to the difficult parameter tuning, it was particularly suitable to suppress the truncation artifacts in the CT type NMR experiments. The simulation and experiments were performed to show the performance of this method. And the processing result was compared with a method proposed recently.
- Nuclear magnetic resonance,
- Sampling truncation,
- Truncation artifacts,
- Artifacts suppression,
- Iterative soft thresholding
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