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Citation: FAN Yong-Mei, ZHANG Ji-Mei, MI Chao, CAI Yu-Ling, ZHANG Li-Ping, ZHU Hai-Bin. Preparation of Polydiallyl Dimethyl Ammonium Chloride Modified Reduced Graphene Oxide/Zinc Oxide Composite Materials and Its Application in Detection of Uric Acid[J]. Chinese Journal of Analytical Chemistry, ;2018, 46(1): 33-38. doi: 10.11895/j.issn.0253-3820.171059 shu

Preparation of Polydiallyl Dimethyl Ammonium Chloride Modified Reduced Graphene Oxide/Zinc Oxide Composite Materials and Its Application in Detection of Uric Acid

The State Key Laboratory of Hollow Fiber Membrane Materials and Processes, Tianjin Polytechnic University, Tianjin 300387, China

Received Date: 3 July 2017
Revised Date: 29 September 2017

Fund Project: This work was supported by the National Natural Science Foundation of China (No. 21106101).

By using zinc nitrate as precursor and hydrazine hydrate as reducing agent, polydiallyl dimethyl ammonium chloride modified reduced graphene oxide/zinc oxide composite materials (PDDA-rGO/ZnO) were prepared by simultaneous reduction of graphene oxide (GO) and zinc nitrate. The composite materials were characterized by Fourier transform infrared (FTIR) spectroscopy, X-ray diffractometer (XRD) and transmission electron microscopy (TEM), and their electrochemical catalytic activity for uric acid was studied by cyclic voltammetry (CV) and linear sweep voltammetry (LSV) measurements. The result showed that PDDA-rGO/ZnO modified glassy carbon electrode prepared here was sensitive, reproducible and stable, and had significant electrocatalytic activity for UA. When using linear sweep voltammetry for detection of UA, the responses of modified electrode were linear with UA concentration in the ranges of 0.02-0.1 mmol/L and 0.1-1.0 mmol/L respectively, with detection limit of 15.9 nmol/L (S/N=3).
- Graphene,
- Zinc oxide,
- Composite material,
- Cyclic voltammetry,
- Linear sweep voltammetry,
- Uric acid
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