Citation: Zhilei Chen, Zhaoxia Li, Yunjiang Yu, Mingdeng Xiang, Cheng Ding, Entian Cui, Jizhou Jiang. Unveiling the enhanced activity origin of BiO_1-xCl/C₃N₅ photocatalyst in CO₂-to-CO directional conversion[J]. Chinese Chemical Letters, ;2026, 37(9): 112313. doi: 10.1016/j.cclet.2025.112313 shu

Unveiling the enhanced activity origin of BiO_1-xCl/C₃N₅ photocatalyst in CO₂-to-CO directional conversion

Zhilei Chen ^a ,
Zhaoxia Li ^a ,
Yunjiang Yu ^b ,
Mingdeng Xiang ^b ,
Cheng Ding ^{a, *,} ,
Entian Cui ^a ,
Jizhou Jiang ^{c, d, *,}

a.
School of Environmental Science and Engineering, Key Laboratory for Advanced Technology in Environmental Protection of Jiangsu Province, Yancheng Institute of Technology Yancheng, Yancheng 224051, China
b.
Key Laboratory of Environmental Pollution Health Risk Assessment, Ministry of Ecology and Environment of the People's Republic of China, South China Institute of Environmental sciences, Guangzhou 510655, China
c.
School of Materials Science and Engineering, State Key Laboratory of Green and Efficient Development of Phosphorus Resources, Engineering Research Center of Phosphorus Resources Development and Utilization of Ministry of Education, Key Laboratory of Green Chemical Engineering Process of Ministry of Education, Hubei Key Laboratory of Plasma Chemistry and Advanced Materials, Novel Catalytic Materials of Hubei Engineering Research Center, Wuhan Institute of Technology, Wuhan 430205, China
d.
College of Chemistry and Molecular Sciences, Wuhan University, Wuhan 430072, China

ycdingc@163.com

027wit@163.com

Received Date: 22 October 2025
Revised Date: 8 December 2025
Accepted Date: 22 December 2025
Available Online: 22 December 2025

Figures(6)

The structure of photocatalysts largely determines the selectivity of CO₂ conversion products in CO₂ photoreduction reaction, while it is dynamic during the photoreaction. Therefore, how the dynamic structure affecting photoactivity deserves further investigation. Herein, with defective oxygen vacancies BiOCl/C₃N₅ nanosheets heterojunction (BiO_1-xCl/C₃N₅) as model photocatalyst, the structure dynamic evolution in CO₂ photoreduction reaction and its influence on the CO₂-to-CO directional conversion were investigated. Specially, in BiO_1-xCl/C₃N₅, the exposed Bi atoms adjected oxygen vacancies interacted with N atoms of C₃N₅ via the strong electrostatic effect, resulting in the shrinking crystalline structures. Once illuminated, the photogenerated electrons enriched on Bi active sites, which further strengthened the interfacial interaction between BiO_1-xCl and C₃N₅ to a quasi-bonding state. The resulting changes in electronic structure destroyed the linear structure of CO₂ molecule pre-adsorbed on Bi sites, accompanying with transformation of Bi atom valence states and heterostructure restoration. As a result, the ^*CO₂ molecule activation and ^*CO intermediate desorption barrier energies both reduced, promoting the CO₂-to-CO directional conversion with a CO evolution rate of 207.3 μmol g⁻¹ h⁻¹. This work demonstrated the importance of studying the structural dynamics evolution in photoreactions, which may be beneficial for future photocatalyst design.
- Photocatalysis,
- CO₂ reduction,
- Composite catalyst,
- Structure dynamic evolution,
- In-situ characterization
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沈阳化工大学材料科学与工程学院沈阳 110142

Unveiling the enhanced activity origin of BiO1-xCl/C3N5 photocatalyst in CO2-to-CO directional conversion

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通讯作者: 陈斌, bchen63@163.com

Unveiling the enhanced activity origin of BiO_1-xCl/C₃N₅ photocatalyst in CO₂-to-CO directional conversion