Citation: Weimei Zeng, Youai Qiu. Electrochemical C-H carboxylation of benzylamines[J]. Chinese Chemical Letters, ;2026, 37(1): 111679. doi: 10.1016/j.cclet.2025.111679 shu

Electrochemical C-H carboxylation of benzylamines

Weimei Zeng ,
Youai Qiu ^*,

State Key Laboratory and Institute of Elemento-Organic Chemistry, Frontiers Science Center for New Organic Matter, Haihe Laboratory of Sustainable Chemical Transformations, College of Chemistry, Nankai University, Tianjin 300071, China

qiuyouai@nankai.edu.cn

Received Date: 16 April 2025
Revised Date: 24 July 2025
Accepted Date: 6 August 2025
Available Online: 7 August 2025

Figures(4)

In this study, electrochemical C-H carboxylation of benzylamines with CO₂ was reported. This linear paired electrolysis system enables efficient and economical synthesis of value-added α-amino acids (α-AAs) under mild conditions. Various substituted benzylamines containing diverse functional groups and even highly reactive moieties, such as cyano, amide and alkene groups could be successfully transformed to the carboxylated products. Notably, this method proved to be applicable to the late-stage modification of biorelevant compounds, highlighting its potential for synthetic chemistry. Mechanistic studies such as radical trapping experiments, kinetic isotope effect (KIE) tests and cyclic voltammetry (CV) studies provided useful insight into this transformation.
- Electrochemical carboxylation,
- Benzylic C-H bond,
- Carbon dioxide,
- α-Amino acids,
- Linear paired electrolysis
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