Citation: Chunxiu Yu, Zelin Wu, Hongle Shi, Lingyun Gu, Kexin Chen, Chuan-Shu He, Yang Liu, Heng Zhang, Peng Zhou, Zhaokun Xiong, Bo Lai. Insights into the electron transfer mechanisms of peroxydisulfate activation by modified metal-free acetylene black for degradation of sulfisoxazole[J]. Chinese Chemical Letters, ;2024, 35(8): 109334. doi: 10.1016/j.cclet.2023.109334 shu

Insights into the electron transfer mechanisms of peroxydisulfate activation by modified metal-free acetylene black for degradation of sulfisoxazole

Chunxiu Yu ^{a, b, c} ,
Zelin Wu ^{a, c} ,
Hongle Shi ^b ,
Lingyun Gu ^{a, b, c, *,} ,
Kexin Chen ^b ,
Chuan-Shu He ^{a, c} ,
Yang Liu ^{a, c} ,
Heng Zhang ^{a, c} ,
Peng Zhou ^{a, c} ,
Zhaokun Xiong ^{a, c, *,} ,
Bo Lai ^{a, c}

a.
State Key Laboratory of Hydraulics and Mountain River Engineering, College of Architecture and Environment, Sichuan University, Chengdu 610065, China
b.
Sichuan Academy of Eco-Environmental Sciences, Chengdu 610041, China
c.
Sino-German Centre for Water and Health Research, Sichuan University, Chengdu 610065, China

glyn0301@126.com

scuxzk@scu.edu.cn

Received Date: 5 September 2023
Revised Date: 19 November 2023
Accepted Date: 22 November 2023
Available Online: 25 November 2023

Figures(7)

Herein, a modified metal-free acetylene black (MMF-AB) catalyst was synthesized by a simple solvothermal-calcination method and designed successfully to activate peroxodisulfate (PDS) for the degradation of sulfisoxazole (SIZ). Due to the doping of N, S and O metal-free elements, the modified catalyst showed excellent catalytic performance with 100% SIZ removal within 30 min. Pseudo first-order reaction rate constants (evaluating catalytic efficiencies and activity) of MMF-AB (k_obs = 0.105 min⁻¹) was 3 times higher than pure-AB (k_obs = 0.029 min⁻¹). Interestingly, it was demonstrated that the reaction system is based on the transfer of electrons from SIZ to PDS to realize an electron-transfer-based mechanism by the evidence of premixing, electron paramagnetic resonance (EPR) spectroscopy, salt-bridge experiments and electrochemical analyses. The introduction of recyclable filtration device solved the secondary pollution caused by the dispersion of the powdered catalyst in the treated water, which further proved the practicality and superiority of the MMF-AB catalyst.
- Peroxydisulfate,
- Sulfisoxazole,
- Acetylene black,
- Electrochemical,
- Electron transfer
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