Citation: Juan Li, Wanling Li, Yan Rao, Feng Shi, Suhua Yu, Huizhen Yang, Lingfeng Min, Zhanjun Yang. Synthesis of highly ordered AgNPs-coated silica photonic crystal beads for sensitive and reproducible 3D SERS substrates[J]. Chinese Chemical Letters, ;2021, 32(1): 150-153. doi: 10.1016/j.cclet.2020.10.043 shu

Synthesis of highly ordered AgNPs-coated silica photonic crystal beads for sensitive and reproducible 3D SERS substrates

Juan Li ^{a, **,} ,
Wanling Li ^a ,
Yan Rao ^a ,
Feng Shi ^a ,
Suhua Yu ^b ,
Huizhen Yang ^a ,
Lingfeng Min ^{c, **,} ,
Zhanjun Yang ^{a, b, *,}

a.
School of Chemistry and Chemical Engineering, Yangzhou University, Yangzhou 225002, China
b.
Guangling College, Yangzhou University, Yangzhou 225002, China
c.
Department of Laboratory Medicine and Clinical Medical College of Yangzhou University, Yangzhou 225001, China

^**

lijuan@yzu.edu.cn

minlingfeng@126.com

zjyang@yzu.edu.cn

Received Date: 14 August 2020
Revised Date: 16 September 2020
Accepted Date: 28 October 2020
Available Online: 29 October 2020

Figures(5)

3D highly ordered silver nanoparticles (AgNPs) coated silica photonic crystal beads (Ag/SPCBs) were prepared and exploited as a novel surface enhanced Raman scattering (SERS) substrate. The monodisperse and size-controlled SPCBs were prepared via self-assembly of silica nanoparticles process using a simple microfluidic device. Then the Ag/SPCBs were easily obtained by in situ growth of AgNPs onto the NH₂-modified SPCBs. Field emitting scanning electron microscopy (SEM) and energy dispersive X-ray spectrometry (EDX) were used to characterize the Ag/SPCBs. The effect of silica nanoparticle size and AgNO₃ concentration on the SERS performance of the resultant Ag/SPCBs substrate were discussed in detail. The results indicate that the Ag/SPCBs have highest SERS signals when silica nanoparticle size is 250 nm and AgNO₃ concentration is 0.8 mg/mL. Using malachite green (MG) as model analyte, the Ag/SPCBs substrate displayed a high sensitivity and a wide linear range for MG. The well-designed Ag/SPCBs show high uniformity and excellent reproducibility, and can be used as an effective SERS substrate for sensitive assay application.
- Surface enhanced Raman scattering,
- Photonic crystal,
- 3D ordered substrate,
- Silver nanoparticles,
- Malachite green
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