Citation: Wang Fang, Huang Anmin, Yin Xiaoqian, Wang Wenshu, Chen Jianbo. Multilevel profiling and identification of Dalbergia odorifera and Dalbergia stevensonii by FTIR, NMR and GC/MS[J]. Chinese Chemical Letters, ;2018, 29(9): 1395-1398. doi: 10.1016/j.cclet.2017.11.007 shu

Multilevel profiling and identification of Dalbergia odorifera and Dalbergia stevensonii by FTIR, NMR and GC/MS

a.
Research Institute of Wood Industry, Chinese Academy of Forestry, Beijing 100091, China
b.
Minzu University of China, Beijing 100081, China
c.
School of Life Sciences, Beijing University of Chinese Medicine, Beijing 100029, China

Corresponding author: Huang Anmin, hbham2000@sina.com Chen Jianbo, chenjianbo@bucm.edu.cn
Received Date: 30 August 2017
Revised Date: 6 November 2017
Accepted Date: 7 November 2017
Available Online: 8 September 2017

Figures(3)

As a rare and valuable wood and herbal material, Dalbergia odorifera is often counterfeited by Dalbergia stevensonii in the market. For the confident chemical identification of D. odorifera and D. stevensonii, the ethanol-benzene extractives are characterized by multiple metabolomics tools, including Fourier transform infrared (FTIR) spectroscopy, nuclear magnetic resonance (NMR), and gas chromatographymass spectrometry (GC/MS). Conventional FTIR spectroscopy, second derivative infrared (SD-IR) spectroscopy and two-dimensional correlation infrared (2D-IR) spectroscopy are combined to interpret the functional groups of the ethanol-benzene extractives. Fingerprint-like characteristics make FTIR a rapid and accurate method to distinguish D. odorifera from D. stevensonii. Chemical differences of the extractives revealed by FTIR methods can be further confirmed by ¹H NMR and ¹³C NMR. Meanwhile, the volatile compounds in the extractives can be identified by GC/MS. The combination of FTIR, NMR and GC/MS makes it possible to obtain the multiple profiles of the ethanol-benzene extractives, which is essential for the confident chemical identification of D. odorifera and D. stevensonii.
- Dalbergia odorifera,
- Dalbergia stevensonii,
- FTIR,
- NMR,
- GC/MS
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1.
沈阳化工大学材料科学与工程学院沈阳 110142