Citation: Hao Xu, Wei Yan, Cheng Li Tang. A novel method to prepare metal oxide electrode:Spin-coating with thermal decomposition[J]. Chinese Chemical Letters, ;2011, 22(3): 354-357. doi: 10.1016/j.cclet.2010.10.027 shu

A novel method to prepare metal oxide electrode:Spin-coating with thermal decomposition

Department of Environmental Science and Technology, Xi'an Jiaotong University, Xi'an 710049, China

Received Date: 9 July 2010

Fund Project: The authors gratefully acknowledge the financial support from the Program for New Century Excellent Talents in University (No. NCET-07-0683), and President Research Fund of Xi'an Jiaotong University (No. 08140016).

In this work, we propose a new spin-coating method coupling with high thermal decomposition, to prepare the tin-antimony (Sn-Sb) oxide electrode. The character of the spin-coating electrode was compared with the dip-coating electrode through X-ray diffraction (XRD), scanning electron microscopy (SEM), accelerated life test, cyclic voltammetry, and electrolytic degradability. The results showed that the spin-coating electrode had a better defined crystal form, a smoother and more compact surface than that of the dip-coating electrode. Service time of the spin-coating electrode was determined to be longer than 15 h, and it was less than 2 min for the dip-coating electrode. Electrochemical characterization analysis showed that the electrolytic degradability of the spin-coating electrode is better than that of the dip-coating electrode.
- Spin-coating,
- Dip-coating,
- Thermal decomposition,
- Electro properties
1. [1]
  Siting Cai , Xiang Chen , Shuli Wang , Xinqin Liao , Zhong Chen , Yue Lin . Silica coating of quantum dots and their applications in optoelectronic fields. Chinese Chemical Letters, 2025, 36(6): 110798-. doi: 10.1016/j.cclet.2024.110798
2. [2]
  Zihe SONG , Jinjin ZHAO , Ning REN , Jianjun ZHANG . Crystal structure, thermal analysis, and luminescence properties of six heterocyclic lanthanide complexes. Chinese Journal of Inorganic Chemistry, 2026, 42(1): 181-192. doi: 10.11862/CJIC.20250126
3. [3]
  Shuai Liang , Wen-Jing Jiang , Ji-Xiang Hu . Achieving colossal anisotropic thermal expansion via synergism of spin crossover and rhombus deformation. Chinese Journal of Structural Chemistry, 2025, 44(2): 100430-100430. doi: 10.1016/j.cjsc.2024.100430
4. [4]
  Yixuan Wang , Jiexin Li , Zhihao Shang , Chengcheng Feng , Jianmin Gu , Maosheng Ye , Ran Zhao , Danna Liu , Jingxin Meng , Shutao Wang . Wettability-driven synergistic resistance of scale and oil on robust superamphiphobic coating. Chinese Chemical Letters, 2024, 35(7): 109623-. doi: 10.1016/j.cclet.2024.109623
5. [5]
  Fengyu Zhang , Yali Liang , Zhangran Ye , Lei Deng , Yunna Guo , Ping Qiu , Peng Jia , Qiaobao Zhang , Liqiang Zhang . Enhanced electrochemical performance of nanoscale single crystal NMC811 modification by coating LiNbO₃. Chinese Chemical Letters, 2024, 35(5): 108655-. doi: 10.1016/j.cclet.2023.108655
6. [6]
  Zeyu XU , Tongzhou LU , Haibo SHAO , Jianming WANG . Preparation and electrochemical lithium storage performance of porous silicon microsphere composite with metal modification and carbon coating. Chinese Journal of Inorganic Chemistry, 2024, 40(10): 1995-2008. doi: 10.11862/CJIC.20240164
7. [7]
  Shilong Li , Ming Zhao , Yefei Xu , Zhanyi Liu , Mian Li , Qing Huang , Xiang Wu . Performance optimization of aqueous Zn/MnO₂ batteries through the synergistic effect of PVP intercalation and GO coating. Chinese Chemical Letters, 2025, 36(3): 110701-. doi: 10.1016/j.cclet.2024.110701
8. [8]
  Bing Jiang , Gang Zou , Bi Luo , Yan Guo , Jingru Li , Wendi Zhang , Qianxiao Fan , Lehao Liu , Lihua Chu , Qiaobao Zhang , Meicheng Li . Enhanced electrochemical performance of lithium-rich layered oxide materials: Exploring advanced coating strategies. Chinese Chemical Letters, 2025, 36(4): 109801-. doi: 10.1016/j.cclet.2024.109801
9. [9]
  Jun-Yang Wang , Yu-Qing Wei , Qing-Ning Wang , Zhi-Guo Wang , Rui Hong , Lisha Yi , Ping Xu , Jia-Zhuang Xu , Zhong-Ming Li , Baisong Zhao . Mucus-inspired lubricative antibacterial coating to reduce airway complications in an intubation cynomolgus monkey model. Chinese Chemical Letters, 2025, 36(8): 110559-. doi: 10.1016/j.cclet.2024.110559
10. [10]
  Sirui Chen , Ran Zhao , Li Dong , Qilin Liu , Wei Chen , Danna Liu , Maosheng Ye , Yingbo Li , Qiong Nie , Jingxin Meng , Shutao Wang . Smart antifouling coating integrating zwitterionic hydrogel with pH-responsive microcapsules for anti-crystal biofilm of orthodontic appliances. Chinese Chemical Letters, 2025, 36(12): 111647-. doi: 10.1016/j.cclet.2025.111647
11. [11]
  Ruotong Wei , Aokun Liu , Jian Kuang , Zhiwen Wang , Lu Yu , Changlin Tian . Probing the dynamic properties in the LLPS process via site-directed spin labeling-electron paramagnetic resonance (SDSL-EPR) spectroscopy. Chinese Chemical Letters, 2025, 36(4): 110029-. doi: 10.1016/j.cclet.2024.110029
12. [12]
  Jiawen Zhu , Yingge Hao , Zhen Song , Huina Zhou , Youmei Wang , Ling Yan , Minghua Lu . Synthesis of mesopore-rich hollow carbon nanospheres as headspace solid-phase microextraction coating to extract PAHs from water and honey. Chinese Chemical Letters, 2025, 36(12): 111290-. doi: 10.1016/j.cclet.2025.111290
13. [13]
  Mingjiao Lu , Zhixing Wang , Gui Luo , Huajun Guo , Xinhai Li , Guochun Yan , Qihou Li , Xianglin Li , Ding Wang , Jiexi Wang . Boosting the performance of LiNi_0.90Co_0.06Mn_0.04O₂ electrode by uniform Li₃PO₄ coating via atomic layer deposition. Chinese Chemical Letters, 2024, 35(5): 108638-. doi: 10.1016/j.cclet.2023.108638
14. [14]
  Bing Niu , Honggao Huang , Liwei Luo , Li Zhang , Jianbo Tan . Coating colloidal particles with a well-defined polymer layer by surface-initiated photoinduced polymerization-induced self-assembly and the subsequent seeded polymerization. Chinese Chemical Letters, 2025, 36(2): 110431-. doi: 10.1016/j.cclet.2024.110431
15. [15]
  Jie Chen , Hannan Chen , Bingbing Tian . Enhancing moisture and electrochemical stability of the Li_5.7PS_4.7Cl_1.3 electrolyte by boron nitride coating for all-solid-state lithium metal batteries. Chinese Chemical Letters, 2025, 36(7): 109775-. doi: 10.1016/j.cclet.2024.109775
16. [16]
  Jiangping Chen , Hongju Ren , Kai Wu , Huihuang Fang , Chongqi Chen , Li Lin , Yu Luo , Lilong Jiang . Boosting hydrogen production of ammonia decomposition via the construction of metal-oxide interfaces. Chinese Journal of Structural Chemistry, 2024, 43(2): 100236-100236. doi: 10.1016/j.cjsc.2024.100236
17. [17]
  Xin Li , Wanting Fu , Ruiqing Guan , Yue Yuan , Qinmei Zhong , Gang Yao , Sheng-Tao Yang , Liandong Jing , Song Bai . Nucleophiles promotes the decomposition of electrophilic functional groups of tetracycline in ZVI/H₂O₂ system: Efficiency and mechanism. Chinese Chemical Letters, 2024, 35(10): 109625-. doi: 10.1016/j.cclet.2024.109625
18. [18]
  Zhen-Zhen Dong , Jin-Hao Zhang , Lin Zhu , Xiao-Zhong Fan , Zhen-Guo Liu , Yi-Bo Yan , Long Kong . Attenuating reductive decomposition of fluorinated electrolytes for high-voltage lithium metal batteries. Chinese Chemical Letters, 2025, 36(4): 109773-. doi: 10.1016/j.cclet.2024.109773
19. [19]
  Hao WANG , Kun TANG , Jiangyang SHAO , Kezhi WANG , Yuwu ZHONG . Electro-copolymerized film of ruthenium catalyst and redox mediator for electrocatalytic water oxidation. Chinese Journal of Inorganic Chemistry, 2024, 40(11): 2193-2202. doi: 10.11862/CJIC.20240176
20. [20]
  Li Li , Zhi-Xin Yan , Chuan-Kun Ran , Yi Liu , Shuo Zhang , Tian-Yu Gao , Long-Fei Dai , Li-Li Liao , Jian-Heng Ye , Da-Gang Yu . Electro-reductive carboxylation of CCl bonds in unactivated alkyl chlorides and polyvinyl chloride with CO₂. Chinese Chemical Letters, 2024, 35(12): 110104-. doi: 10.1016/j.cclet.2024.110104

Get Citation

PDF

XML

Metrics

PDF Downloads(0)
Abstract views(1320)
HTML views(12)

通讯作者: 陈斌, bchen63@163.com

1.
沈阳化工大学材料科学与工程学院沈阳 110142

Address：Zhongguancun North First Street 2,100190 Beijing, PR China Tel: +86-010-82449177-888

DownLoad: Full-Size Img PowerPoint

Return