Citation: Po Yang, Yi Gu. Synthesis of a novel benzoxazine containing benzoxazole structure[J]. Chinese Chemical Letters, ;2010, 21(5): 558-562. doi: 10.1016/j.cclet.2009.12.012 shu

Synthesis of a novel benzoxazine containing benzoxazole structure

Po Yang ,
Yi Gu

State Key Laboratory of Polymer Materials Engineering, College of Polymer Science and Engineering, Sichuan University, Chengdu 610065, China

Received Date: 16 September 2009

Fund Project: This work was supported by the National Natural Science Foundation of China (No. 20774060).

A high-purity benzoxazine (Boz-BOA) containing benzoxazole structure was successfully synthesized by three-step synthetic method using 2-(4-aminophenyl)-1H-benzoxazole-5-amine (BOA) and ortho-hydroxybenzaldehyde. The structure of Boz-BOA was confirmed by FTIR and¹H NMR spectra. The DSC was utilized to probe the curing behavior of Boz-BOA and exhibited a narrow melting peak and curing exothermic peak.
- Benzoxazine,
- Benzoxazole,
- Synthesis,
- Characterization
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