Citation: Hai Feng Sun, Qing Si Zhang, Meng Zhang, Yi Tao Yu, Jian Ping Zong. Synthesis and characterization of α-{3-[2-hydroxy-3-(N-methyl-N-hydroxy-ethylamino)propoxy]propyl}-ω-butylpolydimethylsiloxanes[J]. Chinese Chemical Letters, ;2008, 19(10): 1196-1198. doi: 10.1016/j.cclet.2008.06.047 shu

Synthesis and characterization of α-{3-[2-hydroxy-3-(N-methyl-N-hydroxy-ethylamino)propoxy]propyl}-ω-butylpolydimethylsiloxanes

a School of Chemical Engineering, Shandong Institute of Light Industry, Jinan 250100, China;
b School of Chemistry and Material, Jiangnan University, Wuxi 214122, China

Received Date: 14 April 2008

Fund Project: We gratefully acknowledge the financial support of the Natural Science Foundation of Shandong Province (No. Y2006B22).

α-{3-[2-hydroxy-3-(N-methyl-N-hydroxyethylamino)propoxy]propyl}-ω-butylpolydimethylsiloxanes Ⅲ with various moleculax weights were prepared by epoxy addition of α-[3-(2,3-epoxy-propoxy)propyl]-ω-butylpolydimethylsiloxanes Ⅱ and N-methylmonoethanolamine.At each step.the outcome compounds were characterized through FT-IR and NMR spectra,the results showed that each step was successfully carried out and objective products were achieved.
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