Citation: Qi Zhong Zhou, Chun Lin He, Hai Ning Gu, Qi Ming Miao, Chun Xi Zhai. Convenient synthesis of aryl-incorporated ditosylates and their application in preparation of crown ethers with higher yield[J]. Chinese Chemical Letters, ;2008, 19(8): 911-914. doi: 10.1016/j.cclet.2008.05.038 shu

Convenient synthesis of aryl-incorporated ditosylates and their application in preparation of crown ethers with higher yield

Department of Chemistry, Zhejiang University, Hangzhou 310027, China

Received Date: 7 March 2008

Fund Project: This work was supported by the National Science Foundation (No.DMR0097126).Thanks for good advice from Professor Feihe Huang

A convenient synthetic method with high yields for aryl-incorporated ditosylates by reaction of aryl-incorporated diols with TsCl in THF/NaOH/H₂0 solution was described.Some of these aryl-incorporated ditosylates reacted with diphenols to produce crown ethers in pleasant yield.
- Aryl-incorporated diol,
- Ditosylate,
- Crown ether
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