Citation: Jun Wang, Yibo Wang, Jiran Wu, Dashuang Wang, Cheng Liu, Haiming Huang, Youyong Wang, Chuankun Zhang. Synergizing magnetic exchange resonance and hierarchical dielectric relaxation in multiphase core-shell heterojunctions for efficient microwave dissipation[J]. Acta Physico-Chimica Sinica, ;2026, 42(9): 100336. doi: 10.1016/j.actphy.2026.100336 shu

Synergizing magnetic exchange resonance and hierarchical dielectric relaxation in multiphase core-shell heterojunctions for efficient microwave dissipation

Jun Wang ^{1, 2} ,
Yibo Wang ¹ ,
Jiran Wu ¹ ,
Dashuang Wang ² ,
Cheng Liu ^{1, 2,,} ,
Haiming Huang ¹ ,
Youyong Wang ¹ ,
Chuankun Zhang ^1,,

1.
Hubei Key Laboratory of Energy Storage and Power Battery, Hubei University of Automotive Technology, Shiyan 442002, Hubei Province, China
2.
School of Automotive Materials, Hubei University of Automotive Technology, Shiyan 442002, Hubei Province, China

Corresponding author: Cheng Liu, liuc@huat.edu.cn Chuankun Zhang, zhangchk_lx@huat.edu.cn
Received Date: 23 April 2026
Revised Date: 28 May 2026
Accepted Date: 28 May 2026

Electromagnetic pollution mitigation and radar stealth have driven sustained demand for high-performance broadband microwave absorbing materials. Existing transition-metal-based systems, however, suffer from severe impedance mismatch due to the skin effect, while conventional exogenous oxide-coating strategies improve impedance only at the cost of sacrificing intrinsic magnetic response. To address these limitations, a gradient-controlled thermal oxidation strategy was applied to gas-atomized equiatomic FeCo alloy powder, fabricating FeCo@(Fe,Co)_xO₄ multiphase core-shell heterostructures with continuously tunable oxidation degree. The oxidation degree simultaneously governs core-shell ratio, multiphase shell composition, and interfacial defect states. This in situ topochemical approach preserves the strongly magnetic metallic core for sustained high-frequency magnetic loss, while the derived multiphase semiconducting shell optimizes impedance matching to ensure efficient electromagnetic wave penetration. The incident energy is subsequently dissipated through a synergistic magnetic–dielectric multi-loss mechanism. On one hand, work-function-gradient-induced Mott–Schottky built-in electric fields, combined with oxygen vacancy dipoles and mixed-valence (Fe²⁺/Fe³⁺, Co²⁺/Co³⁺) electron hopping networks, precisely modulate the polarization relaxation time, activating broadband multi-level polarization dissipation across the X-to-Ku band. On the other hand, a high-density interfacial spin-pinning array formed at the rough core-shell heterointerface triggers intense exchange resonance and spin-friction thermal dissipation via the magnetic exchange-spring effect–constituting the dominant attenuation mechanism. Consequently, FeCo-450 achieves RL_min = −60.11 dB and EAB = 7.12 GHz at 1.9 mm, offering important guidance for designing next-generation magnetic metal-based broadband microwave absorbers.
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沈阳化工大学材料科学与工程学院沈阳 110142