Citation: Bo Liang, Yuyijian Zhao, Siyu Wang, Shihan Huang, Fangke Zhou, Chuankun Zhang, Yue Wang, Xiaoming Guo. Synergistic molecular assembly and impedance matching in polyimide-derived porous carbon nanosheets for advanced microwave absorption[J]. Acta Physico-Chimica Sinica, ;2026, 42(6): 100285. doi: 10.1016/j.actphy.2026.100285 shu

Synergistic molecular assembly and impedance matching in polyimide-derived porous carbon nanosheets for advanced microwave absorption

Bo Liang ^{1, 2} ,
Yuyijian Zhao ¹ ,
Siyu Wang ¹ ,
Shihan Huang ¹ ,
Fangke Zhou ¹ ,
Chuankun Zhang ² ,
Yue Wang ^{1, 2,,} ,
Xiaoming Guo ^{1, 2,,}

1.
School of Automotive Materials, Hubei University of Automotive Technology, Shiyan 442002, Hubei Province, China
2.
Hubei Key Laboratory of Energy Storage and Power Battery, School of Optoelectronic Engineering, School of New Energy, Hubei University of Automotive Technology, Shiyan 442002, Hubei Province, China

Corresponding author: Yue Wang, wangyue@huat.edu.cn Xiaoming Guo, gxm@huat.edu.cn
Received Date: 14 February 2026
Revised Date: 10 March 2026
Accepted Date: 11 March 2026

Herein, a novel strategy for fabricating microwave absorption materials via molecular-level design that synergistically regulates dielectric and magnetic losses. The method utilizes a polyimide precursor containing both carboxyl and benzimidazole functional groups as the key component. Through an ice-templating process followed by in-situ ion exchange, Ni²⁺ ions are uniformly incorporated into the polymeric skeleton. Subsequent thermal imidization and carbonization yield nitrogen-doped two-dimensional carbon nanosheets embedded with uniformly dispersed Ni/NiO nanoparticles (BPCN@Ni/NiO). This material exhibits significantly superior microwave absorption properties compared to its counterpart synthesized without the benzimidazole structure (NPCN@Ni/NiO). BPCN@Ni/NiO achieves a remarkable minimum reflection loss (RL_min) of −69.02 dB with effective absorption bandwidth (EAB) of 8.92 GHz (8.28–17.2 GHz). Microstructural analyses confirm its three-dimensional interconnected nanosheet architecture, highly dispersed Ni/NiO species, and homogeneous elemental distribution. The performance enhancement is attributed to the synergistic complexation of Ni²⁺ ions by benzimidazole and carboxyl groups, which enables efficient loading and uniform dispersion of nickel species, thereby optimizing impedance matching. Furthermore, the unique 2D conductive network, abundant heterogeneous interfaces (C/Ni/NiO), defect-induced dipole polarization, and magnetic coupling between Ni and NiO collectively contribute to synergistic multiple loss mechanisms, ultimately endowing the material with excellent microwave attenuation capability. This work offers a new pathway for designing lightweight, efficient, and broadband carbon-based composite absorbers through precise molecular engineering.
- Microwave absorption,
- Benzimidazole polyimide,
- Carbon nanosheets,
- Nickel nanoparticles,
- Heterogeneous interface
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沈阳化工大学材料科学与工程学院沈阳 110142